Determination of lead in whole blood by filter furnace laser-excited atomic fluorescence spectrometry

被引:9
作者
Aucélio, RQ [1 ]
Smith, BW [1 ]
Winefordner, JD [1 ]
机构
[1] Univ Florida, Dept Chem, Gainesville, FL 32611 USA
关键词
filter furnace laser-excited atomic fluorescence spectrometry; blood; lead; calibration curve method;
D O I
10.2116/analsci.15.321
中图分类号
O65 [分析化学];
学科分类号
070302 ; 081704 ;
摘要
Filter furnace laser-excited atomic fluorescence spectroscopy was used for the determination of lead in whole blood. The use of a Katskov filter has enabled the direct comparison between lead fluorescence signals obtained with blood standards and water standards. Only a simple dilution of the blood was required. This direct correlation has allowed the interpolation of the lead signal of blood samples using a lead water standard calibration curve. NIST certified blood samples were analyzed using the method with excellent results.
引用
收藏
页码:321 / 325
页数:5
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