Measurement of J-couplings between spin-1-2 and quadrupolar nuclei by frequency selective solid-state NMR

被引：22

作者：

Amoureux, JP

Trebosc, J

Wiench, JW

Massiot, D

Pruski, M

机构：

[1] Iowa State Univ, Ames Lab, Ames, IA 50011 USA

[2] Univ Lille 1, CNRS 8012, LCPS, F-59652 Villeneuve Dascq, France

[3] CNRS, CRMHT, F-45071 Orleans, France

来源：

SOLID STATE NUCLEAR MAGNETIC RESONANCE | 2005年 / 27卷 / 04期

关键词：

solid-state NMR of quadrupolar nuclei; J-coupling; FS-J-RES; aluminophosphates; VP15;

D O I：

10.1016/j.ssnmr.2004.12.001

中图分类号：

O64 [物理化学（理论化学）、化学物理学];

学科分类号：

070304 ; 081704 ;

摘要：

We report a REDOR-based scheme for the measurement of heteronuclear J-couplings in solid samples with well defined structure, containing spin 1/2 and quadrupolar nuclei, which can be used with selective RF irradiation to target a specific spin pair, and which provides direct information about the number of coupled spins. Published by Elsevier Inc.

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收藏

页码：228 / 232

页数：5

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