Comparison of dry, wet and microwave digestion methods for the multi element determination in some dried fruit samples by ICP-OES

被引:162
作者
Altundag, Huseyin [1 ]
Tuzen, Mustafa [2 ]
机构
[1] Sakarya Univ, Fac Sci & Arts, Dept Chem, TR-54187 Sakarya, Turkey
[2] Gaziosmanpasa Univ, Fac Sci & Arts, Dept Chem, TR-60250 Tokat, Turkey
关键词
Dried fruit; Dry ashing; Wet ashing; Microwave digestion; Trace element; ICP-OES; HEAVY-METALS; WHOLE-BLOOD; SCALP HAIR; CADMIUM; ACCUMULATION; TOXICOLOGY; VARIETIES; ANATOLIA; SPICES; PLANTS;
D O I
10.1016/j.fct.2011.07.064
中图分类号
TS2 [食品工业];
学科分类号
100403 [营养与食品卫生学];
摘要
The aim of this study was used to investigate the level of trace metals (Ba, Pb, Cd, Mn, Cr, Co, Ni, Cu, Mn, Zn, Sr and Fe) in some dried fruits (Prunus domestica L, Fiats carica L, Mortis alba L. Vitis vinifera L., Prunus armeniaca L, and Malus domestica) samples from Turkey. Trace elements were determined by ICP-OES after dry, wet and microwave digestion methods in dried fruit samples. Validation of the proposed method was carried out by using a NIST-SRM 1515-Apple Leaves certified reference material. Element concentrations in dried fruit samples were 0.33-1.77 (Ba). 0.12-0.54 (Cd), 0.25-1.03 (Co), 0.45-2.30 (Cr), 0.43-2.74 (Cu), 0.56-4.87 (Mn), 0.61-2.54 (Ni), 0.40-2.14 (Pb), 2.16-6.54 (Zn), 0.83-12.02 (Al), 11.82-40.80 (Fe) and 0.16-6.34 (Sr) mu g/g. The analytical parameters show that the microwave oven digestion procedure provided best results as compared to the wet and dry digestion procedures. The results were compared with the literature values. (C) 2011 Elsevier Ltd. All rights reserved.
引用
收藏
页码:2800 / 2807
页数:8
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