Mesoporous alumina made from a bicontinuous liquid crystalline phase

被引:11
作者
Cruise, N [1 ]
Jansson, K
Holmberg, K
机构
[1] Chalmers Univ Technol, Dept Appl Surface Chem, SE-41296 Gothenburg, Sweden
[2] Stockholm Univ, Dept Inorgan Chem, SE-10691 Stockholm, Sweden
关键词
monoolein; bicontinuous cubic phase; alumina;
D O I
10.1006/jcis.2001.7811
中图分类号
O64 [物理化学(理论化学)、化学物理学];
学科分类号
070304 ; 081704 ;
摘要
A monoolein-based bicontinuous cubic phase was used as a template for the preparation of a mesoporous alumina. H-1 NMR was used to identify the cubic liquid crystalline region. Transmission electron microscopy images showed the crystallite sizes to be in the range of 3-10 nm and it is these crystallites which appear to be connected with each other in an amorphous matrix in between. The Brunauer-Emmett-Teller specific surface area of the material was 236 m(2)/g and had a pore volume of 0.188 cm(3) g(-1). The material was mainly mesoporous, having an average pore diameter of 38 Angstrom. (C) 2001 Academic Press.
引用
收藏
页码:527 / 529
页数:3
相关论文
共 25 条
[1]   LIQUID-CRYSTALLINE PHASES AS TEMPLATES FOR THE SYNTHESIS OF MESOPOROUS SILICA [J].
ATTARD, GS ;
GLYDE, JC ;
GOLTNER, CG .
NATURE, 1995, 378 (6555) :366-368
[2]   TEMPLATING OF MESOPOROUS MOLECULAR-SIEVES BY NONIONIC POLYETHYLENE OXIDE SURFACTANTS [J].
BAGSHAW, SA ;
PROUZET, E ;
PINNAVAIA, TJ .
SCIENCE, 1995, 269 (5228) :1242-1244
[3]   MOLECULAR OR SUPRAMOLECULAR TEMPLATING - DEFINING THE ROLE OF SURFACTANT CHEMISTRY IN THE FORMATION OF MICROPOROUS AND MESOPOROUS MOLECULAR-SIEVES [J].
BECK, JS ;
VARTULI, JC ;
KENNEDY, GJ ;
KRESGE, CT ;
ROTH, WJ ;
SCHRAMM, SE .
CHEMISTRY OF MATERIALS, 1994, 6 (10) :1816-1821
[4]   A NEW FAMILY OF MESOPOROUS MOLECULAR-SIEVES PREPARED WITH LIQUID-CRYSTAL TEMPLATES [J].
BECK, JS ;
VARTULI, JC ;
ROTH, WJ ;
LEONOWICZ, ME ;
KRESGE, CT ;
SCHMITT, KD ;
CHU, CTW ;
OLSON, DH ;
SHEPPARD, EW ;
MCCULLEN, SB ;
HIGGINS, JB ;
SCHLENKER, JL .
JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1992, 114 (27) :10834-10843
[5]   Syntheses of aluminosilicate mesostructures with high aluminum content [J].
Biz, S ;
White, MG .
JOURNAL OF PHYSICAL CHEMISTRY B, 1999, 103 (40) :8432-8442
[6]  
Cabrera S, 1999, ADV MATER, V11, P379, DOI 10.1002/(SICI)1521-4095(199903)11:5<379::AID-ADMA379>3.0.CO
[7]  
2-6
[8]   In situ ATR/FTIR study of mesoporous silicate syntheses [J].
Calabro, DC ;
Valyocsik, EW ;
Ryan, FX .
MICROPOROUS MATERIALS, 1996, 7 (05) :243-259
[9]   STUDIES ON MESOPOROUS MATERIALS .2. SYNTHESIS MECHANISM OF MCM-41 [J].
CHEN, CY ;
BURKETT, SL ;
LI, HX ;
DAVIS, ME .
MICROPOROUS MATERIALS, 1993, 2 (01) :27-34
[10]   THE NEUTRAL AREA SURFACE OF THE CUBIC MESOPHASE - LOCATION AND PROPERTIES [J].
CHUNG, H ;
CAFFREY, M .
BIOPHYSICAL JOURNAL, 1994, 66 (02) :377-381