Crystal Structure Of Betulin Ethanol Solvate

被引：31

作者：

Drebushchak, T. N. ^{[1
,2
]}

Mikhailenko, M. A. ^{[1
,2
]}

Brezgunova, M. E. ^{[1
,2
]}

Shakhtshneider, T. P. ^{[1
,2
]}

Kuznetsova, S. A. ^{[3
]}

机构：

[1] Russian Acad Sci, Siberian Div, Inst Solid State Chem & Mechanochem, Novosibirsk, Russia

[2] Novosibirsk State Univ, Res & Educ Ctr Mol Design & Ecologically Safe Tec, Novosibirsk, Russia

[3] Russian Acad Sci, Siberian Div, Inst Chem & Chem Technol, Krasnoyarsk, Russia

来源：

JOURNAL OF STRUCTURAL CHEMISTRY | 2010年 / 51卷 / 04期

关键词：

betulin; solvates; hydrogen bond; single crystal X-ray diffraction analysis;

D O I：

10.1007/s10947-010-0121-0

中图分类号：

O61 [无机化学];

学科分类号：

070301 [无机化学];

摘要：

The crystal structure of the 1:1 ethanol betulin solvate, a widely spread natural compound, is determined. The betulin solvate crystallizes in orthorhombic symmetry in the P2(1)2(1)2(1) space group, Z= 4. The unit cell parameters are as follows: a = 7.0159(1) , b = 12.4425(2) , c = 33.7500(5) ; V = 2946.22(8) (3). Betulin molecules are hydrogen bonded to each other and ethanol molecules, as a result of which the layers are distinguished in the structure, which are perpendicular to the crystallographic direction. Inside the layer, all molecules are hydrogen bonded, while the layers are linked by van der Waals interactions.

引用

页码：798 / 801

页数：4

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