Methods of sample preparation for determination of pesticide residues in food matrices by chromatography-mass spectrometry-based techniques: a review

被引:159
作者
Lambropoulou, Dimitra A. [1 ]
Albanis, Triantafyllos A. [1 ]
机构
[1] Univ Ioannina, Dept Chem, Lab Environm Technol, GR-45110 Ioannina, Greece
关键词
pesticides; sample preparation; chromatography-mass spectrometry; food analysis;
D O I
10.1007/s00216-007-1348-2
中图分类号
Q5 [生物化学];
学科分类号
071010 ; 081704 ;
摘要
Much progress has been made in pesticide analysis over the past decade, during which time hyphenated techniques involving highly efficient separation and sensitive detection have become the techniques of choice. Among these, methods based on chromatographic separation with mass spectrometric detection have resulted in greater likelihood of identification and are acknowledged to be extremely useful and authoritative methods for determination of pesticide residues. Even with such powerful instrumental techniques, however, the risk of interference increases with the complexity of the matrix studied, so sample preparation before instrumental analysis is still mandatory in many applications, for example food analysis. This article summarizes the analytical characteristics of the different methods of sample-preparation for determination of pesticide residues in a variety of food matrices, and surveys their recent applications in combination with chromatographic mass spectrometric analysis. We discuss the advantages and the disadvantages of the different methods, address instrumental aspects, and summarize conclusions and perspectives for the future.
引用
收藏
页码:1663 / 1683
页数:21
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