A reaction cell for in situ studies of hydrothermal titration

被引：22

作者：

Norby, P ^{[1
]}

Cahill, C

Koleda, C

Parise, JB

机构：

[1] SUNY Stony Brook, Dept Chem, Stony Brook, NY 11794 USA

[2] SUNY Stony Brook, Dept Earth & Space Sci, Stony Brook, NY 11794 USA

来源：

JOURNAL OF APPLIED CRYSTALLOGRAPHY | 1998年 / 31卷

关键词：

D O I：

10.1107/S002188989701337X

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

A reaction cell for in situ studies of both ion-exchange and hydrothermal titration reactions has been designed and built. This cell allows the injection of reagents into a reaction mixture over time during X-ray data collection. A demonstration experiment followed the injection of Na2SO4(aq) into BaCl2(aq) to yield a time-resolved X-ray powder diffraction pattern of the precipitation of BaSO4(s).

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页码：481 / 483

页数：3

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