An open-flow helium cryostat for single-crystal X-ray diffraction experiments

被引：62

作者：

Hardie, MJ ^{[1
]}

Kirschbaum, K ^{[1
]}

Martin, A ^{[1
]}

Pinkerton, AA ^{[1
]}

机构：

[1] Univ Toledo, Dept Chem, Toledo, OH 43606 USA

来源：

JOURNAL OF APPLIED CRYSTALLOGRAPHY | 1998年 / 31卷

关键词：

D O I：

10.1107/S0021889898003537

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

An open-flow helium cryostat for single-crystal X-ray diffraction experiments capable of reaching 14 K has been developed using off-the-shelf components. Solid/liquid air build-up is prevented using the transfer-line helium back-flow and a heated nozzle. The system has run for over 30 h with no frost build-up.dagger The effectiveness of the system has been demonstrated using test data for oxalic acid, terbium vanadate and dysprosium vanadate.

引用

页码：815 / 817

页数：3

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