4,4′-sulfonylbis[N-(4-nitrophenyl-methylene)benzenamine]:: whole-molecule disorder

被引：8

作者：

Cox, PJ ^{[1
]}

Wardell, JL

机构：

[1] Robert Gordon Univ, Sch Pharm, Aberdeen AB10 1FR, Scotland

[2] Univ Fed Rio de Janeiro, Inst Quim, Dept Quim Inorgan, BR-21945970 Rio De Janeiro, Brazil

来源：

ACTA CRYSTALLOGRAPHICA SECTION C-CRYSTAL STRUCTURE COMMUNICATIONS | 2003年 / 59卷

关键词：

D O I：

10.1107/S0108270103025149

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

The crystal structure of the title compound, C26H18N4O6S, determined from synchrotron data with a small crystal, is characterized by the presence of whole-molecule disorder. In each molecule, the two planar portions are approximately perpendicular to one another and there are short intermolecular contacts between the nitro groups.

引用

页码：O706 / O708

页数：3

共 20 条

[1] The Cambridge Structural Database: a quarter of a million crystal structures and rising [J].

Allen, FH .

ACTA CRYSTALLOGRAPHICA SECTION B-STRUCTURAL SCIENCE, 2002, 58 (3 PART 1) :380-388

[2] SIR97:: a new tool for crystal structure determination and refinement [J].

Altomare, A ;

Burla, MC ;

Camalli, M ;

Cascarano, GL ;

Giacovazzo, C ;

Guagliardi, A ;

Moliterni, AGG ;

Polidori, G ;

Spagna, R .

JOURNAL OF APPLIED CRYSTALLOGRAPHY, 1999, 32 :115-119

[3] MOLECULAR-STRUCTURE AND CRYSTAL PACKING OF 5 4-AMINOPHENYL (4-SUBSTITUTED PHENYL) SULFONES - CORRELATIONS BETWEEN STRUCTURAL DISTORTIONS, SPECTROSCOPIC PARAMETERS AND ELECTRONIC SUBSTITUENT EFFECTS [J].

BERTOLASI, V ;

FERRETTI, V ;

GILLI, P ;

DEBENEDETTI, PG .

JOURNAL OF THE CHEMICAL SOCIETY-PERKIN TRANSACTIONS 2, 1993, (02) :213-219

[4] STEREOCHEMICAL STUDIES OF OLIGOMERS .27. REINVESTIGATION OF THE STRUCTURE OF 4,4'-DIAMINODIPHENYL SULFONE [J].

BOCELLI, G ;

CANTONI, A .

ACTA CRYSTALLOGRAPHICA SECTION C-CRYSTAL STRUCTURE COMMUNICATIONS, 1990, 46 :2257-2259

[5]

*BRIT NAT FORM JOI, 2003, BNF45 JOINT FORM COM

[6]

*BRUK AXS INC, 1998, SADABS VERS 2 03 SAI

[7] A new high-flux chemical and materials crystallography station at the SRS Daresbury .1. Design, construction and test results [J].

Cernik, RJ ;

Clegg, W ;

Catlow, CRA ;

BushnellWye, G ;

Flaherty, JV ;

Greaves, GN ;

Burrows, I ;

Taylor, DJ ;

Teat, SJ ;

Hamichi, M .

JOURNAL OF SYNCHROTRON RADIATION, 1997, 4 :279-286

[8] A novel titanium-oxygen ladder structure supported by calix[4]arene ligands, characterised by synchrotron crystallography [J].

Clegg, W ;

Elsegood, MRJ ;

Teat, SJ ;

Redshaw, C ;

Gibson, VC .

JOURNAL OF THE CHEMICAL SOCIETY-DALTON TRANSACTIONS, 1998, (18) :3037-3039

[9] X-RAY CRYSTAL STRUCTURE OF ANTIMALARIAL AND ANTILEPROTIC DRUG, 4,4' DIAMINODIPHENYL SULPHONE [J].

DICKINSO.C ;

STEWART, JM ;

AMMON, HL .

JOURNAL OF THE CHEMICAL SOCIETY D-CHEMICAL COMMUNICATIONS, 1970, (15) :920-&

[10]

Farrugia L. J., 1999, J. Appl. Crystallogr, V32, P837, DOI [DOI 10.1107/S0021889899006020, 10.1107/S0021889899006020]

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