Synthesis of zeolites NaA and analcime using rice husk ash as silica source without using organic template

被引:78
作者
Azizi, Seyed Naser [1 ]
Yousefpour, Maryam [1 ]
机构
[1] Univ Mazandaran, Fac Chem, Analyt Div, Babol Sar 4741695447, Iran
关键词
MICROWAVE SYNTHESIS; ZSM-5; ZEOLITE; FLY-ASH; MEMBRANES;
D O I
10.1007/s10853-010-4637-7
中图分类号
T [工业技术];
学科分类号
120111 [工业工程];
摘要
Silica was extracted from Fajr rice husk ash (RHA) with approximately 97% purity, converted to sodium and potassium silicate solutions and used as silica source for the synthesis of NaA and analcime zeolites. NaOH and KOH without organic templates were used in the synthesis of NaA and analcime zeolite, respectively. Conventional heating and microwave-assisted hydrothermal were used in zeolite synthesis. Zeolites were characterized with XRD, SEM and IR spectroscopy. Heating time and Si/Al ratio were optimized for the synthesis of zeolites.
引用
收藏
页码:5692 / 5697
页数:6
相关论文
共 19 条
[1]
Synthesis of Aluminum-Rich Analcime Using an Ethylene Diamine Derivative as Template [J].
Azizi, Seyed Naser ;
Yousefpour, Maryam .
ZEITSCHRIFT FUR ANORGANISCHE UND ALLGEMEINE CHEMIE, 2009, 635 (11) :1654-1658
[2]
AZIZI SN, 2001, THESIS U DURHAM
[3]
AZIZI SN, 2008, EURASIAN J ANAL CHEM, V3, P384
[4]
Barrer R.M., 1982, Hydrothermal chemistry of zeolites
[5]
Hydrothermal synthesis of nanostructure NaA zeolite: The effect of synthesis parameters on zeolite seed size and crystallinity [J].
Bayati, B. ;
Babaluo, A. A. ;
Karimi, R. .
JOURNAL OF THE EUROPEAN CERAMIC SOCIETY, 2008, 28 (14) :2653-2657
[6]
Synthesis of ZSM-5 zeolite from lignite fly ash and rice husk ash [J].
Chareonpanich, M ;
Namto, T ;
Kongkachuichay, P ;
Limtrakul, J .
FUEL PROCESSING TECHNOLOGY, 2004, 85 (15) :1623-1634
[7]
Si-29 MAS NMR, XRD and FESEM studies of rice husk silica for the synthesis of zeolites [J].
Hamdan, H ;
Muhid, MNM ;
Endud, S ;
Listiorini, E ;
Ramli, Z .
JOURNAL OF NON-CRYSTALLINE SOLIDS, 1997, 211 (1-2) :126-131
[8]
Microwave-assisted zeolite synthesis from coal fly ash in hydrothermal process [J].
Inada, M ;
Tsujimoto, H ;
Eguchi, Y ;
Enomoto, N ;
Hojo, J .
FUEL, 2005, 84 (12-13) :1482-1486
[9]
A simple method for production of pure silica from rice hull ash [J].
Kalapathy, U ;
Proctor, A ;
Shultz, J .
BIORESOURCE TECHNOLOGY, 2000, 73 (03) :257-262
[10]
Results of thermal and hydrothermal treatment of the aluminosilicate gels prepared at different batch concentrations [J].
Krznaric, I ;
Antonic, T ;
Subotic, B ;
Babic-Ivancic, V .
THERMOCHIMICA ACTA, 1998, 317 (01) :73-84