Preparation of nickel nanopowders in ethanol-water system (EWS)

被引：81

作者：

Zheng, HG ^{[1
]}

Liang, JH

Zeng, JH

Qian, YT

机构：

[1] Univ Sci & Technol China, Dept Chem, Hefei 230026, Anhui, Peoples R China

[2] Univ Sci & Technol China, Struct Res Ctr, Hefei 230026, Anhui, Peoples R China

来源：

MATERIALS RESEARCH BULLETIN | 2001年 / 36卷 / 5-6期

关键词：

metals; nanostructures; chemical synthesis; X-ray diffraction;

D O I：

10.1016/S0025-5408(01)00569-4

中图分类号：

T [工业技术];

学科分类号：

08 ;

摘要：

PVP-protseted nanoscale Ni powders are prepared in ethanol-water system (EWS). The product was characterized by X-ray diffraction (XRD) and transmission electron microscopy (TEM). X-ray photoelectroscopy (XPS) was utilized to determine the surface state of the sample. The product can be isolated in solid state and stabilized for months, The powders are dispersed homogeneously shown in TEM figure, (C) 2001 Elsevier Science Ltd, All rights reserved.

引用

页码：947 / 952

页数：6

共 17 条

[1]

BRADLY JS, 1992, CHEM MATER, V92, P1709

[2]

Chow G M, 1996, ACS SYM SER, P622

[3] Synthesis, characterization, and magnetic studies of nonagglomerated zerovalent iron particles. Unexpected size dependence of the structure [J].

deCaro, D ;

Ould-Ely, T ;

Mari, A ;

Chaudret, B ;

Snoeck, E ;

Respaud, M ;

Broto, JM ;

Fert, A .

CHEMISTRY OF MATERIALS, 1996, 8 (08) :1987-1991

[4] LIGAND STABILIZED NICKEL COLLOIDS [J].

DUTEIL, A ;

SCHMID, G ;

MEYERZAIKA, W .

JOURNAL OF THE CHEMICAL SOCIETY-CHEMICAL COMMUNICATIONS, 1995, (01) :31-32

[5] PREPARATION OF ORGANIC SOLUTIONS OR SOLID FILMS OF SMALL PARTICLES OF RUTHENIUM, PALLADIUM, AND PLATINUM FROM ORGANOMETALLIC PRECURSORS IN THE PRESENCE OF CELLULOSE DERIVATIVES [J].

DUTEIL, A ;

QUEAU, R ;

CHAUDRET, B ;

MAZEL, R ;

ROUCAU, C ;

BRADLEY, JS .

CHEMISTRY OF MATERIALS, 1993, 5 (03) :341-347

[6] SYNTHESIS AND CHARACTERIZATION OF ANISOMETRIC COBALT NANOCLUSTERS [J].

GIBSON, CP ;

PUTZER, KJ .

SCIENCE, 1995, 267 (5202) :1338-1340

[7] SODIUM-BOROHYDRIDE REDUCTION OF COBALT IONS IN NONAQUEOUS MEDIA - FORMATION OF ULTRAFINE PARTICLES (NANOSCALE) OF COBALT METAL [J].

GLAVEE, GN ;

KLABUNDE, KJ ;

SORENSEN, CM ;

HADJIPANAYIS, GC .

INORGANIC CHEMISTRY, 1993, 32 (04) :474-477

[8]

Gonsalves KE, 1996, ACS SYM SER, V622, P220

[9] PROTECTION, SIZE FACTORS, AND REACTION DYNAMICS OF COLLOIDAL REDOX CATALYSTS MEDIATING LIGHT-INDUCED HYDROGEN EVOLUTION FROM WATER [J].

KIWI, J ;

GRATZEL, M .

JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1979, 101 (24) :7214-7217

[10]

KLAUNDE KJ, 1976, J AM CHEM SOC, V98, P1021

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