Metal-organic chemical vapor deposition synthesis of hollow inorganic-fullerene-type MoS2 and MoSe2 nanoparticles

被引：113

作者：

Etzkorn, J

Therese, HA

Rocker, F

Zink, N

Kolb, U

Tremel, W

机构：

[1] Johannes Gutenberg Univ Mainz, Inst Anorgan Chem & Analyt Chem, D-55099 Mainz, Germany

[2] Johannes Gutenberg Univ Mainz, Inst Chem Phys, D-55099 Mainz, Germany

来源：

ADVANCED MATERIALS | 2005年 / 17卷 / 19期

关键词：

D O I：

10.1002/adma.200500850

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

Hollow, nested inorganic fullerene-type MoQ(2) (Q = S, Se) nanoparticles (see Figure) are prepared in high yield and on a large scale from organometallic precursors. The MoQ(2) nanoparticles are obtained by a gas-phase synthesis (using metal-organic chemical vapor deposition) from Mo(CO)(6) and S/Se, followed by a subsequent annealing step.

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页码：2372 / +

页数：5

相关论文

共 30 条

[1] Synthesis of dispersed Mo sulfides in the reactive fluxes containing liquid sulfur and alkali metal carbonates [J].

Afanasiev, P ;

Rawas, L ;

Vrinat, M .

MATERIALS CHEMISTRY AND PHYSICS, 2002, 73 (2-3) :295-300

[2] Electrochemical hydrogen storage in MoS2 nanotubes [J].

Chen, J ;

Kuriyama, N ;

Yuan, H ;

Takeshita, HT ;

Sakai, T .

JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 2001, 123 (47) :11813-11814

[3] Thin films of fullerene-like MoS2 nanoparticles with ultra-low friction and wear [J].

Chhowalla, M ;

Amaratunga, GAJ .

NATURE, 2000, 407 (6801) :164-167

[4] The formation of ReS2 inorganic fullerene-like structures containing Re4 parallelogram units and metal-metal bonds [J].

Coleman, KS ;

Sloan, J ;

Hanson, NA ;

Brown, G ;

Clancy, GP ;

Terrones, M ;

Terrones, H ;

Green, MLH .

JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 2002, 124 (39) :11580-11581

[5]

Dominko R, 2002, ADV MATER, V14, P1531, DOI 10.1002/1521-4095(20021104)14:21<1531::AID-ADMA1531>3.0.CO

[6]

2-P

[7] HIGH-RATE, GAS-PHASE GROWTH OF MOS2 NESTED INORGANIC FULLERENES AND NANOTUBES [J].

FELDMAN, Y ;

WASSERMAN, E ;

SROLOVITZ, DJ ;

TENNE, R .

SCIENCE, 1995, 267 (5195) :222-225

[8] NESTED POLYHEDRA OF MX(2) (M=W, MO X=S, SE) PROBED BY HIGH-RESOLUTION ELECTRON-MICROSCOPY AND SCANNING-TUNNELING-MICROSCOPY [J].

HERSHFINKEL, M ;

GHEBER, LA ;

VOLTERRA, V ;

HUTCHISON, JL ;

MARGULIS, L ;

TENNE, R .

JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1994, 116 (05) :1914-1917

[9] THIN-FILMS OF MOLYBDENUM AND TUNGSTEN DISULFIDES BY METAL ORGANIC-CHEMICAL VAPOR-DEPOSITION [J].

HOFMANN, WK .

JOURNAL OF MATERIALS SCIENCE, 1988, 23 (11) :3981-3986

[10] HELICAL MICROTUBULES OF GRAPHITIC CARBON [J].

IIJIMA, S .

NATURE, 1991, 354 (6348) :56-58