Determination of daminozide in apples and apple leaves by liquid chromatography mass spectrometry

被引：33

作者：

Mol, HGJ ^{[1
]}

van Dam, RCJ ^{[1
]}

Vreeken, RJ ^{[1
]}

Steijger, OM ^{[1
]}

机构：

[1] TNO, Nutr & Food Res Inst, Analyt Sci Div, Dept Pesticides, NL-3700 AJ Zeist, Netherlands

来源：

JOURNAL OF CHROMATOGRAPHY A | 1999年 / 833卷 / 01期

关键词：

apples; fruits; food analysis; daminozide;

D O I：

10.1016/S0021-9673(98)00915-7

中图分类号：

Q5 [生物化学];

学科分类号：

071010 ; 081704 ;

摘要：

A straightforward and efficient method was developed for the determination of intact daminozide in apples and apple leaves. After extraction with methanol and a clean-up step using a graphitized carbon cartridge, the extract was analysed by ion-trap liquid chromatography-tandem mass spectrometry (LC-MS-MS) using atmospheric pressure chemical ionisation in the positive ion mode. Recoveries for apple were 98-102% with a R.S.D.less than or equal to 11% (n = 6) and for leaves were 112-116% with a R.S.D.less than or equal to 18% (n = 6). The limits of detection were 0.008 and 0.02 mg/kg for apples and leaves, respectively. (C) 1999 Elsevier Science B.V. All rights reserved.

引用

页码：53 / 60

页数：8

共 12 条

[1] Determination of daminozide residues in apples using gas chromatography with nitrogen-phosphorus detection [J].

Brinkman, JHW ;

vanDijk, AG ;

Wagenaar, R ;

Quirijns, JK .

JOURNAL OF CHROMATOGRAPHY A, 1996, 723 (02) :355-360

[2]

Clarke S.D., 1996, PHARM SCI, V2, P203

[3] DAMINOZIDE RESIDUE PRESENT IN APPLE FRUIT AFTER LONG AND SHORT-TERM EXPOSURE [J].

DRAKE, SR ;

EISELE, TA ;

BARANOWSKI, JD .

JOURNAL OF FOOD SAFETY, 1991, 11 (04) :247-253

[4]

FAUGHNAN KT, 1991, J ASSOC OFF ANA CHEM, V74, P682

[5]

*GEN INSP HLTH PRO, 1996, AN METH PEST RES FOO

[6]

Kidd H., 1991, AGROCHEMICALS HDB, V3rd

[7] ANALYSIS FOR DAMINOZIDE IN APPLE JUICE BY ANION-EXCHANGE CHROMATOGRAPHY PARTICLE BEAM MASS-SPECTROMETRY [J].

KIM, IS ;

SASINOS, FI ;

STEPHENS, RD ;

BROWN, MA .

JOURNAL OF AGRICULTURAL AND FOOD CHEMISTRY, 1990, 38 (05) :1223-1226

[8]

LUI CH, 1989, J ASSOC OFF ANA CHEM, V72, P984

[9] DETERMINATION OF DAMINOZIDE RESIDUES AT VERY-LOW LEVELS IN FRUITS BY GAS-CHROMATOGRAPHY MASS-SPECTROMETRY [J].

MAJUMDAR, TK ;

GENO, PW ;

YAU, A .

JOURNAL OF AGRICULTURAL AND FOOD CHEMISTRY, 1995, 43 (06) :1421-1423

[10] DETERMINATION OF DAMINOZIDE RESIDUES ON FOODS AND ITS DEGRADATION TO 1,1-DIMETHYLHYDRAZINE BY COOKING [J].

NEWSOME, WH .

JOURNAL OF AGRICULTURAL AND FOOD CHEMISTRY, 1980, 28 (02) :319-321

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