Quantification of micrometre-sized porosity in quasicrystals using coherent synchrotron radiation imaging

被引:15
作者
Agliozzo, S
Cloetens, P
机构
[1] Inst Sci Interchange Fdn, I-10133 Turin, Italy
[2] European Synchrotron Radiat Facil, F-38043 Grenoble, France
关键词
hard X-ray imaging; phase retrieval; porosity; quasicrystals;
D O I
10.1111/j.0022-2720.2004.01385.x
中图分类号
TH742 [显微镜];
学科分类号
摘要
Phase contrast radiography has been applied to investigate porosity in the bulk of quasicrystals. The pores act on X-rays as lenses, leading to drastic changes in the phase contrast images of pores. Depending on the recording conditions and pore features, different imaging regimes are accessed. The variation of the contrast makes the direct characterization of pores from image data, in terms of a precise determination of their size and volume, unreliable. The contrast in Fresnel diffraction images of pores was thus investigated with the support of numerical simulations. A phase retrieval procedure was carried out in order to obtain the correct information from the pore images.
引用
收藏
页码:62 / 69
页数:8
相关论文
共 10 条
[1]   In situ study of the annealing behavior of porosity in icosahedral Al-Pd-Mn quasicrystals using third generation x-ray synchrotron radiation imaging -: art. no. 144204 [J].
Agliozzo, S ;
Gastaldi, J ;
Klein, H ;
Härtwig, J ;
Baruchel, J ;
Brunello, E .
PHYSICAL REVIEW B, 2004, 69 (14) :144204-1
[2]  
Born M., 1986, PRINCIPLES OPTICS
[3]   X-ray diffuse scattering of p-type porous silicon [J].
Buttard, D ;
Bellet, D ;
Dolino, G ;
Baumbach, T .
JOURNAL OF APPLIED PHYSICS, 2002, 91 (05) :2742-2752
[4]   Holotomography: Quantitative phase tomography with micrometer resolution using hard synchrotron radiation x rays [J].
Cloetens, P ;
Ludwig, W ;
Baruchel, J ;
Van Dyck, D ;
Van Landuyt, J ;
Guigay, JP ;
Schlenker, M .
APPLIED PHYSICS LETTERS, 1999, 75 (19) :2912-2914
[5]   Phase objects in synchrotron radiation hard x-ray imaging [J].
Cloetens, P ;
Barrett, R ;
Baruchel, J ;
Guigay, JP ;
Schlenker, M .
JOURNAL OF PHYSICS D-APPLIED PHYSICS, 1996, 29 (01) :133-146
[6]  
Goodman J. W., 1968, INTRO FOURIER OPTICS, P129
[7]  
GUIGAY JP, 1977, OPTIK, V49, P121
[8]   Small angle neutron scattering with single grain quasicrystals [J].
Janot, C ;
de Boissieu, M ;
Agliozzo, S ;
Loreto, L ;
Farinato, R ;
Sato, TJ ;
Tsai, AP ;
Grillo, I .
PHYSICA B, 2001, 300 (1-4) :52-60
[9]  
Koch A., 1999, P 5 INT C INORGANIC, P157
[10]   Investigation of structural defects and inhomogeneities in Al-Pd-Mn icosahedral quasicrystals by combined synchrotron X-ray topography and phase radiography [J].
Mancini, L ;
Reinier, E ;
Cloetens, P ;
Gastaldi, J ;
Härtwig, J ;
Schlenker, M ;
Baruchel, J .
PHILOSOPHICAL MAGAZINE A-PHYSICS OF CONDENSED MATTER STRUCTURE DEFECTS AND MECHANICAL PROPERTIES, 1998, 78 (05) :1175-1194