Development of high-performance liquid chromatographic fingerprint for the quality control of Rheum tanguticum Maxim. ex Balf.

被引:75
作者
Jin, Wei
Ge, Ri-Li
Wei, Quan-Jia
Bao, Tian-You
Shi, Hai-Ming
Tu, Peng-Fei [1 ]
机构
[1] Peking Univ, Ctr Hlth Sci, Sch Pharmaceut Sci, Beijing 100083, Peoples R China
[2] Qinghai Univ, Coll Med, Xining 810001, Peoples R China
关键词
high-performance liquid chromatographic fingerprint; quality control; Rheum tanguticum; traditional Chinese medicine (TCM);
D O I
10.1016/j.chroma.2006.08.022
中图分类号
Q5 [生物化学];
学科分类号
071010 [生物化学与分子生物学]; 081704 [应用化学];
摘要
A novel, accurate and valid fingerprint method was developed by using high-performance liquid chromatography-photodiode array detection (HPLC-DAD) to control the quality of Rheum tanguticum Maxim. ex Balf. By comprehensively comparing chromatograms of all samples, our result, revealed that the chromatographic fingerprint we developed combining similarity evaluation could efficiently identify and distinguish raw materials of R. tanguticum from different sources. Besides, 21 characteristic peaks in chromatogram of R. tanguticum were unambiguously confirmed by comparison of reference compounds based on their retention time (t(R)) and UV spectra. (c) 2006 Elsevier B.V. All rights reserved.
引用
收藏
页码:320 / 324
页数:5
相关论文
共 11 条
[1]
[Anonymous], 1991, Guidelines for the Assessment of Herbal Medicines
[2]
FRIEDRICH H, 1967, KHIM PRIV SOEDUN, V3, P646
[3]
Quality evaluation of fingerprints of herbal medicine with chromatographic data [J].
Li, BY ;
Hu, Y ;
Liang, YZ ;
Xie, PS ;
Du, YP .
ANALYTICA CHIMICA ACTA, 2004, 514 (01) :69-77
[4]
LOU ZC, 1993, J BEIJING MED U, V30, P3
[5]
Development of high-performance liquid chromatographic fingerprints for distinguishing Chinese Angelica from related umbelliferae herbs [J].
Lu, GH ;
Chan, K ;
Liang, YZ ;
Leung, K ;
Chan, CL ;
Jiang, ZH ;
Zhao, ZZ .
JOURNAL OF CHROMATOGRAPHY A, 2005, 1073 (1-2) :383-392
[6]
NONAKA GI, 1977, CHEM PHARM BULL, V25, P2300
[7]
*STAT PHARM COMM P, 2005, PHARM PR CHIN, P17
[8]
Fingerprint analysis of Flos Carthami by capillary electrophoresis [J].
Sun, Y ;
Guo, T ;
Sui, Y ;
Li, F .
JOURNAL OF CHROMATOGRAPHY B-ANALYTICAL TECHNOLOGIES IN THE BIOMEDICAL AND LIFE SCIENCES, 2003, 792 (02) :147-152
[9]
XIE PS, 2005, CHROMATOGRAPHIC FING, P469
[10]
Fingerprint quality control of Tianjihuang by high-performance liquid chromatography-photodiode array detection [J].
Yang, LW ;
Wu, DH ;
Tang, X ;
Peng, W ;
Wang, XR ;
Ma, Y ;
Su, WW .
JOURNAL OF CHROMATOGRAPHY A, 2005, 1070 (1-2) :35-42