Synthesis and characterization of Ni magnetic nanoparticles in AlMCM41 host

被引：25

作者：

Jung, JS ^{[1
]}

Choi, KH

Chae, WS

Kim, YR

Jun, JH

Malkinski, L

Kodenkandath, T

Zhou, WL

Wiley, JB

O'Connor, CJ

机构：

[1] Kangnung Natl Univ, Dept Chem, Kangnung 210702, South Korea

[2] Yonsei Univ, Dept Chem, Seoul 120749, South Korea

[3] Konkuk Univ, Dept Appl Chem, Chungju 380701, South Korea

[4] Polish Acad Sci, Inst Phys, Warsaw, Poland

[5] Univ New Orleans, Adv Mat Res Inst, New Orleans, LA 70148 USA

来源：

JOURNAL OF PHYSICS AND CHEMISTRY OF SOLIDS | 2003年 / 64卷 / 03期

关键词：

nickel nanoparticles; MCM41; transmission electron microscopy; X-ray diffraction; magnetic properties;

D O I：

10.1016/S0022-3697(02)00279-2

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

Superparamagnetic nickel nanoparticles were prepared by incorporating nickel ion into A1MCM41 as a nanoreactor and then reduced with sodium borohydride or H-2 gas. Products were characterized by elemental analysis, transmission electron microscopy, X-ray powder diffraction, and magnetic susceptibility. The nickel particle size and blocking temperature depend on the reduction method. (C) 2002 Elsevier Science Ltd. All rights reserved.

引用

页码：385 / 390

页数：6

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