Soft X-ray spectromicroscopy for in situ study of corrosion

被引:10
作者
Kurtis, KE
Meyer-Ilse, W
Monteiro, PJM
机构
[1] Georgia Inst Technol, Sch Civil & Environm Engn, Atlanta, GA 30332 USA
[2] Univ Calif Berkeley, Lawrence Berkeley Lab, Ctr Xray Opt, Berkeley, CA 94720 USA
[3] Univ Calif Berkeley, Dept Civil & Environm Engn, Berkeley, CA 94720 USA
关键词
steel; iron; oxidation; microscopy;
D O I
10.1016/S0010-938X(99)00147-X
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
Corrosion of filings from an ASTM Grade 60 steel reinforcing bar was examined in situ using the soft X-ray transmission microscope XM-1, operated by the Center for X-ray Optics and located at the Advanced Light Source at E.O. Lawrence Berkeley National Laboratory. Iron distribution maps generated from X-ray images of a steel filing before and after the addition of water show the change in elemental iron distribution in the sample. The decreased presence of iron in the distribution map after the introduction of water indicates the oxidation of iron - the anodic reaction in steel corrosion. These results demonstrate the utility of transmission soft X-ray microscopy for in, situ corrosion studies. (C) 2000 Elsevier Science Ltd. All rights reserved.
引用
收藏
页码:1327 / 1336
页数:10
相关论文
共 12 条
  • [1] Fickelhorn M, 1990, MAT STRUCTURES J RIL, V23, P317
  • [2] CORE-LEVEL BINDING-ENERGIES IN METALS
    FUGGLE, JC
    MARTENSSON, N
    [J]. JOURNAL OF ELECTRON SPECTROSCOPY AND RELATED PHENOMENA, 1980, 21 (03) : 275 - 281
  • [4] HECK JM, 1998, XRAY MICROSCOPY SPEC, pII130
  • [5] Kurtis KE, 1999, J MICROSC-OXFORD, V196, P288
  • [6] Imaging of ASR gel by soft X-ray microscopy
    Kurtis, KE
    Monteiro, PJM
    Brown, JT
    Meyer-Ilse, W
    [J]. CEMENT AND CONCRETE RESEARCH, 1998, 28 (03) : 411 - 421
  • [7] KURTIS KE, 1997, P CANMET ACI INT C D, P535
  • [8] Intracellular structures of normal and aberrant Plasmodium falciparum malaria parasites imaged by soft x-ray microscopy
    Magowan, C
    Brown, JT
    Liang, J
    Heck, J
    Coppel, RL
    Mohandas, N
    MeyerIlse, W
    [J]. PROCEEDINGS OF THE NATIONAL ACADEMY OF SCIENCES OF THE UNITED STATES OF AMERICA, 1997, 94 (12) : 6222 - 6227
  • [9] Meyer-Ilse W., 1998, XRAY MICROSCOPY SPEC
  • [10] MEYERILSE W, 1995, SYNCHR RAD NEWS, V8, P29