Ordered mesoporous silica and alumina thin films studied by X-ray scattering

被引:6
作者
Klotz, M [1 ]
Idrissi-Kandri, N [1 ]
Ayral, A [1 ]
van der Lee, A [1 ]
Guizard, C [1 ]
机构
[1] Univ Montpellier 2, UMR 5635 CNRS, Inst Europeen Membranes, F-34095 Montpellier 5, France
来源
JOURNAL DE PHYSIQUE IV | 2002年 / 12卷 / PR6期
关键词
D O I
10.1051/jp4:20020237
中图分类号
O4 [物理学];
学科分类号
0702 ;
摘要
The use of X-ray techniques for the characterisation of ordered mesoporous films is demonstrated. Both silica and alumina thin layers with an ordered mesoporosity are studied using low-angle diffraction and grazing incidence reflectometry. It is shown how the internal structure evolves upon drying and how texture can be easily detected using a two-circle diffractometer. The reflectometry data are correlated with results from nitrogen adsorption/desorption experiments.
引用
收藏
页码:283 / 289
页数:7
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