X-ray powder diffraction study of the thermal behavior of barium titanium citrate hydrate

被引:4
作者
Louer, D [1 ]
Criado, JM [1 ]
Dianez, MJ [1 ]
Perez-Maqueda, LA [1 ]
机构
[1] CSIC, INST CIENCIA MAT, SEVILLE 41092, SPAIN
关键词
D O I
10.1017/S0885715600009684
中图分类号
TB3 [工程材料学];
学科分类号
0805 ; 080502 ;
摘要
The thermal decomposition of barium bis(citrato)oxolitanate citrate heptahydrate, a molecular precursor of BaTiO3 fine powders is studied by temperature-dependent x-ray powder diffraction and thermogravimetry. A thorough investigation of the dehydration stage is presented. Three crystalline phases containing seven, three, and two water molecules, respectively, are identified from their powder diffraction pattern. The results of pattern indexing are presented and discussed in terms of parameter relationships. (C) 1997 International Centre for Diffraction Data.
引用
收藏
页码:180 / 184
页数:5
相关论文
共 10 条
[1]   INDEXING OF POWDER DIFFRACTION PATTERNS FOR LOW-SYMMETRY LATTICES BY THE SUCCESSIVE DICHOTOMY METHOD [J].
BOULTIF, A ;
LOUER, D .
JOURNAL OF APPLIED CRYSTALLOGRAPHY, 1991, 24 (pt 6) :987-993
[2]   SYNTHESIS AND CHARACTERIZATION OF BATI(OC6H5)(6)CENTER-DOT(2)DMF, A SINGLE-SOURCE SOL-GEL PRECURSOR TO BATIO3 GELS, POWDERS, AND THIN-FILMS [J].
DAY, VW ;
EBERSPACHER, TA ;
KLEMPERER, WG ;
LIANG, S .
CHEMISTRY OF MATERIALS, 1995, 7 (09) :1607-1608
[3]   THERMAL-DECOMPOSITION OF (BATI) CITRATES INTO BARIUM-TITANATE [J].
HENNINGS, D ;
MAYR, W .
JOURNAL OF SOLID STATE CHEMISTRY, 1978, 26 (04) :329-338
[4]  
HUTCHINS GA, 1987, AM CERAM SOC BULL, V66, P681
[5]   PEAK SHAPE AND RESOLUTION IN CONVENTIONAL DIFFRACTOMETRY WITH MONOCHROMATIC X-RAYS [J].
LOUER, D ;
LANGFORD, JI .
JOURNAL OF APPLIED CRYSTALLOGRAPHY, 1988, 21 :430-437
[6]  
LOUER D, 1990, POWDER DIFFR, V5, P162
[7]   CRYSTAL-STRUCTURE OF BARIUM TITANYL OXALATE BATIO(C2O4)2.4.5H2O [J].
LOUER, M ;
LOUER, D ;
GOTOR, FJ ;
CRIADO, JM .
JOURNAL OF SOLID STATE CHEMISTRY, 1991, 92 (02) :565-572
[8]  
PECHINI MP, 1961, Patent No. 2985506
[9]   TIME-RESOLVED STUDY BY X-RAY-POWDER DIFFRACTION WITH POSITION-SENSITIVE DETECTOR - RATE OF THE BETA-CS2CDL4 TRANSFORMATION AND THE EFFECT OF PREFERRED ORIENTATION [J].
PLEVERT, J ;
AUFFREDIC, JP ;
LOUER, M ;
LOUER, D .
JOURNAL OF MATERIALS SCIENCE, 1989, 24 (06) :1913-1918
[10]   FORMATION OF BATIO3 FROM CITRATE PRECURSOR [J].
RAJENDRAN, M ;
RAO, MS .
JOURNAL OF SOLID STATE CHEMISTRY, 1994, 113 (02) :239-247