Small-angle neutron scattering from samples of expanded carbon

被引:7
作者
Bogdanov, S. G.
Valiev, E. Z.
Dorofeev, Yu. A.
Pirogov, A. N.
Skryabin, Yu. N.
Makotchenko, V. G.
Nazarov, A. S.
Fedorov, V. E.
机构
[1] Russian Acad Sci, Ural Div, Inst Met Phys, Ekaterinburg 620041, Russia
[2] Russian Acad Sci, Inst Inorgan Chem, Siberian Div, Novosibirsk 630090, Russia
关键词
61.12.-g;
D O I
10.1134/S1063774506070030
中图分类号
O7 [晶体学];
学科分类号
0702 ; 070205 ; 0703 ; 080501 ;
摘要
The subatomic structure of expanded graphite has been investigated by small-angle neutron scattering. Samples were synthesized during quick thermal decomposition of intercalated compounds based on oxidized graphite. They had a low bulk density (up to 0.1 g/cm(3)) and were characterized by considerable small-angle scattering. It has been established that majority of the volume of expanded graphite samples is occupied by participles with characteristic sizes in two ranges: from 6 to 8 nm and from 20 to 30 nm. Small particles have properties of a surface fractal with the dimension D-s = 2.4-2.6, whereas the larger particles are mainly smooth and have the dimension D-s = 2.0-2.1. The specific surface of the samples studied was determined from the small-angle scattering data.
引用
收藏
页码:S12 / S15
页数:4
相关论文
共 10 条
  • [1] SMALL-ANGLE X-RAY-SCATTERING INVESTIGATION OF SUBMICROSCOPIC POROSITY WITH FRACTAL PROPERTIES
    BALE, HD
    SCHMIDT, PW
    [J]. PHYSICAL REVIEW LETTERS, 1984, 53 (06) : 596 - 599
  • [2] SCATTERING BY AN INHOMOGENEOUS SOLID .2. THE CORRELATION FUNCTION AND ITS APPLICATION
    DEBYE, P
    ANDERSON, HR
    BRUMBERGER, H
    [J]. JOURNAL OF APPLIED PHYSICS, 1957, 28 (06) : 679 - 683
  • [3] Lukashin AV, 1999, DOKL AKAD NAUK+, V369, P781
  • [4] X-RAY POWDER DIFFRACTION STUDY OF POLY(CARBON MONOFLUORIDE), CF1.12
    MAHAJAN, VK
    BADACHHAPE, RB
    MARGRAVE, JL
    [J]. INORGANIC & NUCLEAR CHEMISTRY LETTERS, 1974, 10 (12): : 1103 - 1109
  • [5] Nazarov A. S., 2002, IAN SSSR NEORG MATER, V38, P351
  • [6] SCHAEFER DW, 1988, FRACTALS PHYS
  • [7] Svergun D. I., 1986, XRAY NEUTRON SMALL A
  • [8] Structural state of expanded graphite prepared from intercalation compounds
    Teplykh, A. E.
    Bogdanov, S. G.
    Dorofeev, Yu. A.
    Pirogov, A. N.
    Skryabin, Yu. N.
    Makotchenko, V. G.
    Nazarov, A. S.
    Fedorov, V. E.
    [J]. CRYSTALLOGRAPHY REPORTS, 2006, 51 (Suppl 1) : S62 - S66
  • [9] Valiev E. Z., 2002, POVERKHNOST, P59
  • [10] Valiev E. Z., 2001, POVERKHNOST, P38