GC-MS Analysis of the Essential Oil of Coral Ginger (Zingiber corallinum Hance) Rrhizome Obtained by Supercritical Fluid Extraction and Steam Distillation Extraction

被引:30
作者
Yang Zhannan [1 ]
Luo Shiqiong [2 ]
Peng Quancai [1 ,2 ]
Zhao Chao [1 ]
Yu Zhengwen [2 ]
机构
[1] Guizhou Normal Univ, Key Lab Informat Syst Mountainous, Area & Protect Ecol Environm Guizhou Province, Guiyang 550001, Guizhou, Peoples R China
[2] Guizhou Normal Univ, Sch Biotechnol & Engn, Guiyang 550001, Guizhou, Peoples R China
关键词
Gas chromatography-mass spectrometry; Supercritical fluid extraction; Steam distillation extraction; Zingiber corallinum Hance; CARBON-DIOXIDE EXTRACTION; VOLATILE; CONSTITUENTS;
D O I
10.1365/s10337-009-0971-9
中图分类号
Q5 [生物化学];
学科分类号
070307 [化学生物学];
摘要
The chemical compositions of volatile oils extracted from Zingiber corallinum Hance were obtained by steam distillation extraction (SDE) and supercritical fluid extraction (SFE) followed by gas chromatography-mass spectrometry analysis. The effects of pressure, temperature, modifier volume, and extraction time on the SFE of Z. corallinum oil were investigated, and optimization of the conditions were: extraction temperature, 30 A degrees C; dynamic extraction time, 40 min; pressure, 10 Mpa; and modifier volume, 50 mL. 29 compounds from SFE extracts were identified. The main components were sabinene (16.19%), terpinen-4-ol (16.26%), beta-sesquiphellandrene (3.26%), triquinacene 1, 4-bis (methoxy) (22.01%), triquinacene 1,4,7-tris (methoxy) (3.66%), 1-[4-(1-methyl-2-propenyl) phenyl] ethanone (9.87%) and ferulic acid methyl ester (16.88%) accounting for 88.13% of all compounds. SFE extracts were found to be markedly different from the corresponding SDE extracts. 22 compounds from SDE extracts were identified. The major components, accounting for 92.48% of SDE extracts, were sabinene (53.38%), alpha-terpinene (3.23%), gamma-terpinen (2.16%), terpinen-4-ol (22.66%), beta-sesquiphellandrene (1.41%) and triquinacene, 1, 4-bis (methoxy) (9.64%).
引用
收藏
页码:785 / 790
页数:6
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