Chiral separation of racemic thiols based on diastereomer formation with a fluorescent chiral tagging reagent by reversed-phase liquid chromatography

被引：13

作者：

Jin, DR ^{[1
]}

Takehana, K ^{[1
]}

Toyooka, T ^{[1
]}

机构：

[1] UNIV SHIZUOKA, SCH PHARMACEUT SCI, DEPT ANALYT CHEM, YADA, SHIZUOKA 422, JAPAN

来源：

ANALYTICAL SCIENCES | 1997年 / 13卷 / 01期

关键词：

racemic thiol; precolumn derivatization; diastereomer formation; fluorescence detection; reversed-phase liquid chromatography;

D O I：

10.2116/analsci.13.113

中图分类号：

O65 [分析化学];

学科分类号：

070302 ; 081704 ;

摘要：

[No abstract available]

引用

页码：113 / 115

页数：3

共 11 条

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[2] RESOLUTION OF THE ENANTIOMERS OF THIOL COMPOUNDS BY REVERSED-PHASE LIQUID-CHROMATOGRAPHY USING CHIRAL DERIVATIZATION WITH 2,3,4,6-TETRA-O-ACETYL-BETA-D-GLUCOPYRANOSYL ISOTHIOCYANATE
ITO, S
OTA, A
YAMAMOTO, K
KAWASHIMA, Y
[J]. JOURNAL OF CHROMATOGRAPHY, 1992, 626 (02): : 187 - 196
[3] KRSTULOVIC AM, 1989, CHIRAL SEPARATION HP
[4] OPTICAL RESOLUTION OF THIOL ENANTIOMERS BY HIGH-PERFORMANCE LIQUID-CHROMATOGRAPHY USING PRECOLUMN FLUORESCENCE DERIVATIZATION WITH O-PHTHALALDEHYDE AND ALPHA-AMINO-ACIDS
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[J]. ANALYTICAL SCIENCES, 1995, 11 (02) : 299 - 301
[5] CHIRAL SEPARATION BY HIGH-PERFORMANCE LIQUID-CHROMATOGRAPHY .1. REVIEW ON INDIRECT SEPARATION OF ENANTIOMERS AS DIASTEREOMERIC DERIVATIVES USING ULTRAVIOLET, FLUORESCENCE AND ELECTROCHEMICAL DETECTION
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[J]. BIOMEDICAL CHROMATOGRAPHY, 1992, 6 (04) : 163 - 167
[6] DEVELOPMENT OF OPTICALLY-ACTIVE FLUORESCENT EDMAN-TYPE REAGENTS
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LIU, YM
[J]. ANALYST, 1995, 120 (02) : 385 - 390
[7] Toyooka T, 1996, BIOMED CHROMATOGR, V10, P265, DOI 10.1002/(SICI)1099-0801(199611)10:6<265::AID-BMC602>3.0.CO
[8] 2-A
[9] Sequential analysis of D/L-amino acid in peptide with a novel chiral Edman degradation method
Toyooka, T
Suzuki, T
Watanabe, T
Liu, YM
[J]. ANALYTICAL SCIENCES, 1996, 12 (05) : 779 - 782
[10] HIGH-PERFORMANCE LIQUID-CHROMATOGRAPHIC RESOLUTION OF AMINO-ACID ENANTIOMERS DERIVATIZED WITH FLUORESCENT CHIRAL EDMAN REAGENTS
TOYOOKA, T
LIU, YM
[J]. JOURNAL OF CHROMATOGRAPHY A, 1995, 689 (01) : 23 - 30

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