Synthesis and characterization of ultrafine CeO2 particles by glycothermal process

被引:44
作者
Bae, DS [1 ]
Lim, B
Kim, BI
Han, KS
机构
[1] Korea Inst Sci & Technol, Div Ceram, Seoul 136791, South Korea
[2] Korea Inst Ceram Engn & Technol, Dept Ceram, Seoul 2335, South Korea
关键词
ultrafine CeO2; glycothermal process; ethylene glycol; KOH;
D O I
10.1016/S0167-577X(02)00563-3
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
The cerium oxide nanosize particles were prepared under mild temperature and pressure conditions by precipitation from metal nitrates with aqueous potassium hydroxide. Various types of cerium oxide powders were obtained at 200-230degreesC. The average size of synthesized particles was in the range of 10-50 nm and the phase of synthesized particles was crystalline. The effects of synthesis parameters, such as the concentration of starting solution, pH of starting solution, reaction temperature and time, are discussed. (C) 2002 Elsevier Science B.V. All tights reserved.
引用
收藏
页码:610 / 613
页数:4
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