Two-step in situ annealing effects on sputter-deposited MgB2 thin films

被引:13
作者
Mori, Z [1 ]
Doi, T
Eitoku, K
Ishizaki, Y
Kitaguchi, H
Okada, M
Saitoh, K
Hakuraku, Y
机构
[1] Yatsushiro Natl Tech Coll, Kumamoto 8668501, Japan
[2] Kagoshima Univ, Fac Engn, Kagoshima 8900065, Japan
[3] NIMS, Tsukuba, Ibaraki 3050047, Japan
[4] Hitachi Ltd, Hitachi Res Lab, Hitachi, Ibaraki 3191292, Japan
[5] Hitachi Ltd, Adv Res Lab, Kokubunji, Tokyo 1858601, Japan
关键词
D O I
10.1088/0953-2048/17/1/008
中图分类号
O59 [应用物理学];
学科分类号
摘要
We have investigated the effects of in situ annealing on the superconducting C properties of MgB2 thin films for the purpose of obtaining high critical temperature close to bulk value. MgB2 thin films were fabricated by rf magnetron sputtering on C-plane sapphire (Al2O3) substrate. Thin films In were produced by simultaneously sputtering pure B and a Mg metal target. Sputtering deposition was followed by in situ annealing in a high vacuum. To prevent the evaporation of Mg from the film surface, two-step annealing p C, was adopted: the first step is the crystallization stage at low-temperature annealing and the next is an improvement of the film's superconducting properties by annealing at a high temperature. In the optimal annealing process (a thin film is first heated at 600 degreesC for 2 It and then 650 degreesC for 2 h) we have consistently obtained thin films with a zero resistivity temperature of 29 K.
引用
收藏
页码:47 / 50
页数:4
相关论文
共 19 条
[1]   Superconducting Mg-B films by pulsed-laser deposition in an in situ two-step process using multicomponent targets [J].
Blank, DHA ;
Hilgenkamp, H ;
Brinkman, A ;
Mijatovic, D ;
Rijnders, G ;
Rogalla, H .
APPLIED PHYSICS LETTERS, 2001, 79 (03) :394-396
[2]   Superconducting thin films of MgB2 on Si by pulsed laser deposition [J].
Brinkman, A ;
Mijatovic, D ;
Rijnders, G ;
Leca, V ;
Smilde, HJH ;
Oomen, I ;
Golubov, AA ;
Roesthuis, F ;
Harkema, S ;
Hilgenkamp, H ;
Blank, DHA ;
Rogalla, H .
PHYSICA C-SUPERCONDUCTIVITY AND ITS APPLICATIONS, 2001, 353 (1-2) :1-4
[3]   Vaporization thermodynamics of MgB2 and MgB4 [J].
Brutti, S ;
Ciccioli, A ;
Balducci, G ;
Gigli, G ;
Manfrinetti, P ;
Palenzona, A .
APPLIED PHYSICS LETTERS, 2002, 80 (16) :2892-2894
[4]   Superconducting magnesium diboride films with Tc ≈ 24 K grown by pulsed laser deposition with in situ anneal [J].
Christen, HM ;
Zhai, HY ;
Cantoni, C ;
Paranthaman, M ;
Sales, BC ;
Rouleau, C ;
Norton, DP ;
Christen, DK ;
Lowndes, DH .
PHYSICA C-SUPERCONDUCTIVITY AND ITS APPLICATIONS, 2001, 353 (3-4) :157-161
[5]   Experimental study of MgB2 decomposition [J].
Fan, ZY ;
Hinks, DG ;
Newman, N ;
Rowell, JM .
APPLIED PHYSICS LETTERS, 2001, 79 (01) :87-89
[6]   Superconducting MgB2 thin films prepared by chemical vapor deposition from diborane [J].
Fu, XH ;
Wang, DS ;
Zhang, ZP ;
Yang, J .
PHYSICA C-SUPERCONDUCTIVITY AND ITS APPLICATIONS, 2002, 377 (04) :407-410
[7]   In situ growth of superconducting MgB2 thin films with preferential orientation by molecular-beam epitaxy [J].
Jo, W ;
Huh, JU ;
Ohnishi, T ;
Marshall, AF ;
Beasley, MR ;
Hammond, RH .
APPLIED PHYSICS LETTERS, 2002, 80 (19) :3563-3565
[8]   Growth of superconducting MgB2 thin films via postannealing techniques [J].
Kang, WN ;
Choi, EM ;
Kim, HJ ;
Kim, HJ ;
Lee, S .
PHYSICA C-SUPERCONDUCTIVITY AND ITS APPLICATIONS, 2003, 385 (1-2) :24-30
[9]   Negligible effect of grain boundaries on the supercurrent density in polycrystalline MgB2 [J].
Kim, KHP ;
Kang, WN ;
Kim, MS ;
Jung, CU ;
Kim, HJ ;
Choi, EM ;
Park, MS ;
Lee, SI .
PHYSICA C-SUPERCONDUCTIVITY AND ITS APPLICATIONS, 2002, 370 (01) :13-16
[10]   Superconducting properties of MgB2 thin films prepared on flexible plastic substrates [J].
Kús, P ;
Plecenik, A ;
Satrapinsky, L ;
Xu, Y ;
Sobolewski, R .
APPLIED PHYSICS LETTERS, 2002, 81 (12) :2199-2201