Hollow magnetite spheres: Synthesis, characterization, and magnetic properties

被引：84

作者：

Chen, XY ^{[1
]}

Zhang, ZJ ^{[1
]}

Li, XX ^{[1
]}

Shi, CW ^{[1
]}

机构：

[1] Hefei Univ Technol, Sch Chem Engn, Hefei 230009, Anhui, Peoples R China

来源：

CHEMICAL PHYSICS LETTERS | 2006年 / 422卷 / 1-3期

关键词：

D O I：

10.1016/j.cplett.2006.02.082

中图分类号：

O64 [物理化学（理论化学）、化学物理学];

学科分类号：

070304 ; 081704 ;

摘要：

Magnetite (Fe3O4) hollow spheres have been synthesized in ethylene glycol (EG) solution without adding any additives, using FeCl3 center dot 6H(2)O and urea as the starting materials. The experimental results reveal that the solvent and reaction temperature have the important influences on the phase and morphology of the products based on XRD and TEM characterization. The magnetic properties of magnetite hollow spheres exhibit a ferromagnetic behavior according to the magnetic hysteresis curve measured at room temperature. It is noticeable that beta-FeOOH nanorods and alpha-Fe2O3 nanocrystallites can be selectively fabricated by adjusting the reaction solvents. (c) 2006 Elsevier B.V. All rights reserved.

引用

页码：294 / 298

页数：5

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