Selected-control synthesis of PbO2 submicrometer-sized hollow spheres and Pb3O4 microtubes

被引:62
作者
Xi, GC
Peng, YY
Xu, LQ
Zhang, M
Yu, WC
Qian, YT [1 ]
机构
[1] Univ Sci & Technol China, Struct Res Lab, Hefei 230026, Anhui, Peoples R China
[2] Univ Sci & Technol China, Dept Chem, Hefei 230026, Anhui, Peoples R China
基金
中国国家自然科学基金;
关键词
hollow spheres; microtubes; lead oxides; electrodes;
D O I
10.1016/j.inoche.2004.03.001
中图分类号
O61 [无机化学];
学科分类号
070301 ; 081704 ;
摘要
Submicrometer-sized PbO2 hollow spheres and Pb3O4 microtubes were prepared by a selected-control synthesis method for the first time. The diameter of the PbO2 hollow spheres is about 200-400 nm and the wall thickness is about 30-50 nm. The Pb3O4 microtubes with tetragonal cross-section are 15-20 mum in length, 3-4 mum in width, and 0.4-0.6 mum in wall thickness. The experimental results indicated that poly(vinyl pyrrolidone) (PVP) plays a unique role in controlling the morphologies of lead oxides. (C) 2004 Elsevier B.V. All rights reserved.
引用
收藏
页码:607 / 610
页数:4
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