High resolution and high fields in biological solid state NMR

被引：13

作者：

Cotten, M

Soghomonian, VG

Hu, W

Cross, TA

机构：

[1] FLORIDA STATE UNIV,INST MOL BIOPHYS,NATL HIGH MAGNET FIELD LAB,TALLAHASSEE,FL 32306

[2] FLORIDA STATE UNIV,DEPT CHEM,TALLAHASSEE,FL 32306

来源：

SOLID STATE NUCLEAR MAGNETIC RESONANCE | 1997年 / 9卷 / 01期

基金：

美国国家科学基金会;

关键词：

high resolution; high fields; biological solid state NMR;

D O I：

10.1016/S0926-2040(97)00046-5

中图分类号：

O64 [物理化学（理论化学）、化学物理学];

学科分类号：

070304 ; 081704 ;

摘要：

H-2 solid state NMR spectra of a polypeptide in an oriented membrane environment is demonstrated to have an orientational resolution of 0.3 degrees. Such data results in high resolution structural constraints. Similar spectra are demonstrated at 23.2 T using a resistive magnet at the National High Magentic Field Laboratory. (C) 1997 Elsevier Science B.V.

引用

页码：77 / 80

页数：4

共 12 条

[1] Andrew E.R., 1969, J MAGN RESON, V1969, P27
[2] NUCLEAR MAGNETIC RESONANCE SPECTRA FROM A CRYSTAL ROTATED AT HIGH SPEED
ANDREW, ER
BRADBURY, A
EADES, RG
[J]. NATURE, 1958, 182 (4650) : 1659 - 1659
[3] Direct determination of a molecular torsional angle by solid-state NMR
Feng, X
Lee, YK
Sandstrom, D
Eden, M
Maisel, H
Sebald, A
Levitt, MH
[J]. CHEMICAL PHYSICS LETTERS, 1996, 257 (3-4) : 314 - 320
[4] DEUTERIUM NMR OF VAL1...(2-H-2)ALA3...GRAMICIDIN-A IN ORIENTED DMPC BILAYERS
HING, AW
ADAMS, SP
SILBERT, DF
NORBERG, RE
[J]. BIOCHEMISTRY, 1990, 29 (17) : 4144 - 4156
[5] TRYPTOPHAN DYNAMICS AND STRUCTURAL REFINEMENT IN A LIPID BILAYER ENVIRONMENT - SOLID-STATE NMR OF THE GRAMICIDIN CHANNEL
HU, W
LAZO, ND
CROSS, TA
[J]. BIOCHEMISTRY, 1995, 34 (43) : 14138 - 14146
[6] Ketchem RR, 1996, J BIOMOL NMR, V8, P1
[7] HIGH-RESOLUTION CONFORMATION OF GRAMICIDIN-A IN A LIPID BILAYER BY SOLID-STATE NMR
KETCHEM, RR
HU, W
CROSS, TA
[J]. SCIENCE, 1993, 261 (5127) : 1457 - 1460
[8] Distance measurements in nucleic acids using windowless dipolar recoupling solid state NMR
Mehta, MA
Gregory, DM
Kiihne, S
Mitchell, DJ
Hatcher, ME
Shiels, JC
Drobny, GP
[J]. SOLID STATE NUCLEAR MAGNETIC RESONANCE, 1996, 7 (03) : 211 - 228
[9] MOLL F, 1988, THESIS FLORIDA STATE
[10] CORRELATIONS BETWEEN FUNCTION AND DYNAMICS - TIME-SCALE COINCIDENCE FOR ION TRANSLOCATION AND MOLECULAR-DYNAMICS IN THE GRAMICIDIN CHANNEL BACKBONE
NORTH, CL
CROSS, TA
[J]. BIOCHEMISTRY, 1995, 34 (17) : 5883 - 5895

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