Synthesis of monodisperse and spherical YAG nanopowder by a mixed solvothermal method

被引:75
作者
Zhang, XD [1 ]
Liu, H
He, W
Wang, HY
Li, X
Boughton, RI
机构
[1] Shandong Univ, State Key Lab Crystal Mat, Jinan 250100, Peoples R China
[2] Shandong Inst Light Ind, Dept Mat Sci & Engn, Jinan 250100, Peoples R China
[3] Bowling Green State Univ, Ctr Mat Sci, Bowling Green, OH 43403 USA
关键词
nanostructures; chemical synthesis; nanofabrications; X-ray diffraction;
D O I
10.1016/j.jallcom.2003.10.010
中图分类号
O64 [物理化学(理论化学)、化学物理学];
学科分类号
070304 ; 081704 ;
摘要
Yttrium aluminum garnet (YAG) powder was synthesized by a mixed solvothermal method under milder conditions with inexpensive aluminum and yttrium nitrates as the starting materials, and the low-cost ethanol-water mixed solution as the solvent. X-ray diffraction (XRD), DTA and TEM analysis showed that the powder synthesized was single-phase YAG, with well-dispersed fine spherical grains (80 nm average) and a relatively narrow grain size distribution. Moreover, the crystallization process of YAG grains was discussed. (C) 2003 Elsevier B.V. All rights reserved.
引用
收藏
页码:300 / 303
页数:4
相关论文
共 24 条
[1]   Barium titanate powders synthesis from solvothermal reaction and supercritical treatment [J].
Bocquet, JF ;
Chhor, K ;
Pommier, C .
MATERIALS CHEMISTRY AND PHYSICS, 1999, 57 (03) :273-280
[2]  
CORMAN GS, 1991, CERAM ENG SCI P, V12, P1745
[3]  
DAWSON WJ, 1988, AM CERAM SOC BULL, V67, P1673
[4]   Preparation of titania particles by thermal hydrolysis of TiCl4 in n-propanol solution [J].
Fang, CS ;
Chen, YW .
MATERIALS CHEMISTRY AND PHYSICS, 2003, 78 (03) :739-745
[5]   SYNTHESIS OF YTTRIUM ALUMINATES BY THE SOL-GEL PROCESS [J].
GOWDA, G .
JOURNAL OF MATERIALS SCIENCE LETTERS, 1986, 5 (10) :1029-1032
[6]   Production of phosphor (YAG:Tb) fine particles by hydrothermal synthesis in supercritical water [J].
Hakuta, Y ;
Seino, K ;
Ura, H ;
Adschiri, T ;
Takizawa, H ;
Arai, K .
JOURNAL OF MATERIALS CHEMISTRY, 1999, 9 (10) :2671-2674
[7]   Synthesis and optical properties of Nd3+-doped Y3Al5O12 nanoceramics [J].
Hreniak, D ;
Strek, W .
JOURNAL OF ALLOYS AND COMPOUNDS, 2002, 341 (1-2) :183-186
[8]   FABRICATION AND OPTICAL-PROPERTIES OF HIGH-PERFORMANCE POLYCRYSTALLINE ND-YAG CERAMICS FOR SOLID-STATE LASERS [J].
IKESUE, A ;
KINOSHITA, T ;
KAMATA, K ;
YOSHIDA, K .
JOURNAL OF THE AMERICAN CERAMIC SOCIETY, 1995, 78 (04) :1033-1040
[9]   FABRICATION OF POLYCRYSTALLINE, TRANSPARENT YAG CERAMICS BY A SOLID-STATE REACTION METHOD [J].
IKESUE, A ;
FURUSATO, I ;
KAMATA, K .
JOURNAL OF THE AMERICAN CERAMIC SOCIETY, 1995, 78 (01) :225-228
[10]   SYNTHESIS OF YTTRIUM-ALUMINUM-GARNET BY THE GLYCOTHERMAL METHOD [J].
INOUE, M ;
OTSU, H ;
KOMINAMI, H ;
INUI, T .
JOURNAL OF THE AMERICAN CERAMIC SOCIETY, 1991, 74 (06) :1452-1454