The BioCAT undulator beamline 18ID: a facility for biological non-crystalline diffraction and X-ray absorption spectroscopy at the Advanced Photon Source

被引:128
作者
Fischetti, R
Stepanov, S
Rosenbaum, G
Barrea, R
Black, E
Gore, D
Heurich, R
Kondrashkina, E
Kropf, AJ
Wang, S
Zhang, K
Irving, TC
Bunker, GB
机构
[1] IIT, Dept Biol Chem & Phys Sci, Biophys Collaborat Access Team, Chicago, IL 60616 USA
[2] Univ Georgia, SER CAT, Athens, GA 30602 USA
[3] Argonne Natl Lab, CMT Div, Argonne, IL 60439 USA
关键词
X-ray beamlines; non-crystalline diffraction; small-angle X-ray scattering; X-ray absorption spectroscopy; XAFS; XANES; EXAFS;
D O I
10.1107/S0909049504016760
中图分类号
TH7 [仪器、仪表];
学科分类号
0804 ; 080401 ; 081102 ;
摘要
The 18ID undulator beamline of the Biophysics Collaborative Access Team at the Advanced Photon Source, Argonne, IL, USA, is a high-performance instrument designed for, and dedicated to, the study of partially ordered and disordered biological materials using the techniques of small-angle X-ray scattering, fiber diffraction, and X-ray absorption spectroscopy. The beamline and associated instrumentation are described in detail and examples of the representative experimental results are presented.
引用
收藏
页码:399 / 405
页数:7
相关论文
共 34 条
[1]   Design of a vacuum-compatible high-precision monochromatic beam-position monitor for use with synchrotron radiation from 5 to 25 keV [J].
Alkire, RW ;
Rosenbaum, G ;
Evans, G .
JOURNAL OF SYNCHROTRON RADIATION, 2000, 7 (02) :61-68
[2]   Low-resolution structures of proteins in solution retrieved from X-ray scattering with a genetic algorithm [J].
Chacón, P ;
Morán, F ;
Díaz, JF ;
Pantos, E ;
Andreu, JM .
BIOPHYSICAL JOURNAL, 1998, 74 (06) :2760-2775
[3]  
CRAMER SP, 1988, XRAY ABSORPTION, P257
[4]  
Dejus R., 1994, TECHNICAL B ANL APS, V17
[5]   High-resolution wide-angle X-ray scattering of protein solutions: effect of beam dose on protein integrity [J].
Fischetti, RF ;
Rodi, DJ ;
Mirza, A ;
Irving, TC ;
Kondrashkina, E ;
Makowski, L .
JOURNAL OF SYNCHROTRON RADIATION, 2003, 10 :398-404
[6]   Fiber diffraction using the BioCAT undulator beamline at the Advanced Photon Source [J].
Irving, T.C. ;
Fischetti, R. ;
Rosenbaum, G. ;
Bunker, G.B. .
Nuclear Instruments and Methods in Physics Research, Section A: Accelerators, Spectrometers, Detectors and Associated Equipment, 2000, 448 (01) :250-254
[7]   In vivo X-ray diffraction of indirect flight muscle from Drosophila melanogaster [J].
Irving, TC ;
Maughan, DW .
BIOPHYSICAL JOURNAL, 2000, 78 (05) :2511-2515
[8]  
IRVING TC, 2001, FIBRE DIFFR REV, V9, P58
[9]  
Ivanov I, 2000, AIP CONF PROC, V521, P271, DOI 10.1063/1.1291799
[10]   Early collapse is not an obligate step in protein folding [J].
Jacob, J ;
Krantz, B ;
Dothager, RS ;
Thiyagarajan, P ;
Sosnick, TR .
JOURNAL OF MOLECULAR BIOLOGY, 2004, 338 (02) :369-382