In-situ, non-destructive identification of chemical elements by means of portable EDXRF spectrometer

被引:18
作者
Fiorini, C [1 ]
Longoni, A [1 ]
机构
[1] Politecn Milan, Dipartimento Elettron & Informaz, I-20133 Milan, Italy
关键词
D O I
10.1109/23.819273
中图分类号
TM [电工技术]; TN [电子技术、通信技术];
学科分类号
0808 ; 0809 ;
摘要
The performances of a new portable EDXRF (Energy Dispersive X-ray Fluorescence) Spectrometer designed for insitu, non-destructive identification of chemical elements in materials are here described. The instrument, based on a Silicon Drift Detector cooled by a Peltier element, does not require a liquid nitrogen cooling system. The energy resolution of the spectrometer is typically 155 eV FWHM at 6 keV at a temperature of about -8 degrees C and the peak to valley ratio is better than 10000. The paper reports on the most significant results recently obtained, by using a new version of the Silicon Drift Detector, in measurements carried out "on-the-field" on samples of different materials. The results of the first quantitative analyses of metal alloys carried out with this instrument are also presented.
引用
收藏
页码:2011 / 2016
页数:6
相关论文
共 11 条
[1]   Applications of non-cryogenic portable EDXRF systems in archaeometry [J].
Cesareo, R ;
Gigante, GE ;
Canegallo, P ;
Castellano, A ;
Iwanczyk, JS ;
Dabrowski, A .
NUCLEAR INSTRUMENTS & METHODS IN PHYSICS RESEARCH SECTION A-ACCELERATORS SPECTROMETERS DETECTORS AND ASSOCIATED EQUIPMENT, 1996, 380 (1-2) :440-445
[2]   A new detection system for x-ray microanalysis based on a silicon drift detector with Peltier cooling [J].
Fiorini, C ;
Kemmer, J ;
Lechner, P ;
Kromer, K ;
Rohde, M ;
Schulein, T .
REVIEW OF SCIENTIFIC INSTRUMENTS, 1997, 68 (06) :2461-2465
[3]   Application of a new noncryogenic x-ray detector in portable instruments for archaeometric analyses [J].
Fiorini, C ;
Longoni, A .
REVIEW OF SCIENTIFIC INSTRUMENTS, 1998, 69 (03) :1523-1528
[4]   SEMICONDUCTOR DRIFT CHAMBER - AN APPLICATION OF A NOVEL CHARGE TRANSPORT SCHEME [J].
GATTI, E ;
REHAK, P .
NUCLEAR INSTRUMENTS & METHODS IN PHYSICS RESEARCH SECTION A-ACCELERATORS SPECTROMETERS DETECTORS AND ASSOCIATED EQUIPMENT, 1984, 225 (03) :608-614
[5]   Ultrathin entrance windows for silicon drift detectors [J].
Hartmann, R ;
Struder, L ;
Kemmer, J ;
Lechner, P ;
Fries, O ;
Lorenz, E ;
Mirzoyan, R .
NUCLEAR INSTRUMENTS & METHODS IN PHYSICS RESEARCH SECTION A-ACCELERATORS SPECTROMETERS DETECTORS AND ASSOCIATED EQUIPMENT, 1997, 387 (1-2) :250-254
[6]   HIGH-PERFORMANCE, THERMOELECTRICALLY COOLED X-RAY AND GAMMA-RAY DETECTORS [J].
HUBER, AC ;
PANTAZIS, JA ;
JORDANOV, V .
NUCLEAR INSTRUMENTS & METHODS IN PHYSICS RESEARCH SECTION B-BEAM INTERACTIONS WITH MATERIALS AND ATOMS, 1995, 99 (1-4) :665-668
[7]   PERFORMANCE AND DURABILITY OF HGI2 X-RAY-DETECTORS FOR SPACE MISSIONS [J].
IWANCZYK, JS ;
WANG, YJ ;
BRADLEY, JG ;
CONLEY, JM ;
ALBEE, AL ;
ECONOMOU, TE .
IEEE TRANSACTIONS ON NUCLEAR SCIENCE, 1989, 36 (01) :841-845
[8]  
KEMMER J, 1999, IN PRESS NUCL INSTR
[9]   FUNDAMENTAL ALGORITHM BETWEEN CONCENTRATION AND INTENSITY IN XRF ANALYSIS .1. THEORY [J].
ROUSSEAU, RM .
X-RAY SPECTROMETRY, 1984, 13 (03) :115-120
[10]  
SCIUTI S, 1991, RIV NUOVO CIMENTO, V14