Crystallization of MFI and MEL zeolites from clear solutions

被引:20
作者
Testa, F
Szostak, R
Chiappetta, R
Aiello, R
Fonseca, A
Nagy, JB
机构
[1] UNIV CALABRIA,DIPARTIMENTO INGN CHIM & MAT,CALABRIA,ITALY
[2] CLARK ATLANTA UNIV,DEPT CHEM,ATLANTA,GA 30314
[3] FAC UNIV NOTRE DAME PAIX,LAB RMN,B-5000 NAMUR,BELGIUM
来源
ZEOLITES | 1997年 / 18卷 / 2-3期
关键词
synthesis; clear solution; MFI structure; MEL structure; characterization; (XRD; SEM; dtg-dta; FT-IR; multi NMR);
D O I
10.1016/S0144-2449(96)00133-9
中图分类号
O64 [物理化学(理论化学)、化学物理学];
学科分类号
070304 ; 081704 ;
摘要
Pure MFI and MEL zeolites were obtained at 170 degrees C from clear solutions of general composition SiO2: 0.0004 Al2O3: 0.30 Na2O : aTAABr (or TAAOH) : 40H(2)O with a = 0.03 -0.16 and TAA = TEA, TPA or TEA. The physicochemical characteristics (XRD, SEM, d.t.g., d.t.a., FT i.r., and multi-n.m.r.) allow one to compare the products obtained from the clear solution with those obtained from a hydrogel. (C) Elsevier Science Inc. 1997.
引用
收藏
页码:106 / 114
页数:9
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