Preparation and characterization of Y2O3 hollow spheres

被引：9

作者：

Han, Chunrui ^{[1
]}

Wu, Xiuyong ^{[1
]}

Lin, Yusheng ^{[1
]}

Gu, Guohua ^{[1
]}

Fu, Xun ^{[1
]}

Hi, Zhengshui ^{[1
]}

机构：

[1] Qingdao Univ Sci & Technol, Qingdao 266042, Shandong, Peoples R China

来源：

JOURNAL OF MATERIALS SCIENCE | 2006年 / 41卷 / 12期

关键词：

D O I：

10.1007/s10853-006-6296-2

中图分类号：

T [工业技术];

学科分类号：

08 ;

摘要：

Y2O3 hollow spheres are prepared by coating the anionic poly (styrene-methyl acrylic acid) (PSA-A) latex with an amorphous yttrium layer and subsequent calcining at elevated temperatures in air. The aging temperature, aging time, the concentrations of Y(III) and urea are systematically varied to establish the optimum conditions for the formation of the coating shell. Zeta potential measurement, transmission electron microscopy, scanning electron microscopy, X-ray diffraction and infrared measurements are used to characterize the PSA-A latex, core-shell spheres and Y2O3 hollow spheres. A mechanism for the formation of the PSA-A/yttrium compounds core-shell spheres is suggested. The key factor to prepare smooth-coated spheres is obtained. (c) 2006 Springer Science + Business Media, Inc.

引用

页码：3679 / 3682

页数：4

共 13 条

[1] PREPARATION AND PROPERTIES OF MONODISPERSED COLLOIDAL PARTICLES OF LANTHANIDE COMPOUNDS .3. YTTRIUM(III) AND MIXED YTTRIUM(III)-CERIUM(III) SYSTEMS [J].

AIKEN, B ;

HSU, WP ;

MATIJEVIC, E .

JOURNAL OF THE AMERICAN CERAMIC SOCIETY, 1988, 71 (10) :845-853

[2] New solid and hollow, magnetic and non-magnetic, organic-inorganic monodispersed hybrid microspheres: synthesis and characterization [J].

Bamnolker, H ;

Nitzan, B ;

Gura, S ;

Margel, S .

JOURNAL OF MATERIALS SCIENCE LETTERS, 1997, 16 (16) :1412-1415

[3] Multilayered titania, silica, and Laponite nanoparticle coatings on polystyrene colloidal templates and resulting inorganic hollow spheres [J].

Caruso, RA ;

Susha, A ;

Caruso, F .

CHEMISTRY OF MATERIALS, 2001, 13 (02) :400-409

[4] Ceramic hollow spheres and their applications [J].

Cochran, JK .

CURRENT OPINION IN SOLID STATE & MATERIALS SCIENCE, 1998, 3 (05) :474-479

[5]

[郭玉 Guo Yu], 2003, [高分子材料科学与工程, Polymer Materials Science & Engineering], V19, P40

[6] PREPARATION OF HOLLOW SPHERICAL-PARTICLES OF YTTRIUM COMPOUNDS [J].

KAWAHASHI, N ;

MATIJEVIC, E .

JOURNAL OF COLLOID AND INTERFACE SCIENCE, 1991, 143 (01) :103-110

[7] PREPARATION AND PROPERTIES OF UNIFORM COATED COLLOIDAL PARTICLES .5. YTTRIUM BASIC CARBONATE ON POLYSTYRENE LATEX [J].

KAWAHASHI, N ;

MATIJEVIC, E .

JOURNAL OF COLLOID AND INTERFACE SCIENCE, 1990, 138 (02) :534-542

[8]

Lu Y, 2001, ADV MATER, V13, P271, DOI 10.1002/1521-4095(200102)13:4<271::AID-ADMA271>3.3.CO

[9]

2-K

[10] Titanium compounds as coatings on polystyrene latices and as hollow spheres [J].

Shiho, H ;

Kawahashi, N .

COLLOID AND POLYMER SCIENCE, 2000, 278 (03) :270-274

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