Synthesis and characterization of MgF2 and KMgF3 nanorods

被引:59
作者
Cao, MH
Wang, YH
Qi, YJ
Guo, CX
Hu, CW [1 ]
机构
[1] NE Normal Univ, Fac Chem, Inst Polyoxometalate Chem, Changchun 130024, Peoples R China
[2] Beijing Inst Technol, Dept Chem, Beijing 100081, Peoples R China
基金
高等学校博士学科点专项科研基金; 中国国家自然科学基金;
关键词
one-dimensional nanostructures; MgF2; KMgF3; microemulsion; hydrothermal reactions;
D O I
10.1016/j.jssc.2004.01.005
中图分类号
O61 [无机化学];
学科分类号
070301 ; 081704 ;
摘要
MgF2 nanorods with diameters of 60-100 nm were synthesized by a microemulsion method. Subsequent hydrothermal reaction of as-synthesized MgF2 nanorods and KF at 240degreesC for 3 days or 140degreesC for 7 days resulted in KMgF3 nanorods, which retained the rod-like morphology of the source material MgF2 in the reaction process. The morphology of as-synthesized MgF2 strongly depended on the molar ratio between water and the surfactant CTAB and the concentration of CTAB. (C) 2004 Elsevier Inc. All rights reserved.
引用
收藏
页码:2205 / 2209
页数:5
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