Study of a polymer immobilized on silica gel as stationary phase for chiral liquid chromatography

被引：11

作者：

Guillaume, M

Sebille, B

机构：

[1] Lab. de Physchim. des Biopolymeres, UMR 27 CNRS-Univ. Paris XII, F-94320 Thiais

来源：

EUROPEAN POLYMER JOURNAL | 1996年 / 32卷 / 01期

关键词：

D O I：

10.1016/0014-3057(95)00120-4

中图分类号：

O63 [高分子化学（高聚物）];

学科分类号：

070305 ; 080501 ; 081704 ;

摘要：

The adsorption of beta-cyclodextrin polymer was studied on different silica beads, in water-organic solvent mixtures. A maximum adsorption on Lichrospher 100 Angstrom 5 mu m was observed for a polymer solution containing 70% acetone. Different crosslinking agents were used to stabilize the polymer layer on the silica surface to make a convenient support for liquid chromatography. Glutaraldehyde appeared as very efficient for this purpose and enabled chiral supports to be prepared.

引用

页码：19 / 26

页数：8

共 35 条

[1] [Anonymous], STARCH
[2] A NOVEL POLYVIOLOGEN ELECTRODE FABRICATED BY ELECTROCHEMICAL CROSS-LINKING
CHANG, HC
OSAWA, M
MATSUE, T
UCHIDA, I
[J]. JOURNAL OF THE CHEMICAL SOCIETY-CHEMICAL COMMUNICATIONS, 1991, (09) : 611 - 612
[3] CLASSIFICATION OF THE SOLUBILITY BEHAVIOR OF BETA-CYCLODEXTRIN IN AQUEOUS COSOLVENT MIXTURES
COLEMAN, AW
MUNOZ, M
CHATJIGAKIS, AK
CARDOT, P
[J]. JOURNAL OF PHYSICAL ORGANIC CHEMISTRY, 1993, 6 (12) : 651 - 659
[4] INTERACTION BETWEEN ASYMMETRIC SOLUTES AND SOLVENTS - N-LAUROYL-L-VALYL TERT BUTYLAMIDE AS STATIONARY PHASE IN GAS LIQUID PARTITION CHROMATOGRAPHY
FEIBUSH, B
[J]. JOURNAL OF THE CHEMICAL SOCIETY D-CHEMICAL COMMUNICATIONS, 1971, (11): : 544 - &
[5] GILAV E, 1966, TETRAHEDRON LETT, P1009
[6] THIN-LAYER CHROMATOGRAPHIC-SEPARATION OF ORTHO, META, AND PARA-SUBSTITUTED BENZOIC-ACIDS AND PHENOLS WITH AQUEOUS-SOLUTIONS OF ALPHA-CYCLODEXTRIN
HINZE, WL
ARMSTRONG, DW
[J]. ANALYTICAL LETTERS PART A-CHEMICAL ANALYSIS, 1980, 13 (12): : 1093 - 1104
[7] LIQUID-CHROMATOGRAPHIC SEPARATION OF ENANTIOMERS USING A CHIRAL BETA-CYCLODEXTRIN-BONDED STATIONARY PHASE AND CONVENTIONAL AQUEOUS ORGANIC MOBILE PHASES
HINZE, WL
RIEHL, TE
ARMSTRONG, DW
DEMOND, W
ALAK, A
WARD, T
[J]. ANALYTICAL CHEMISTRY, 1985, 57 (01) : 237 - 242
[8] (1S,2R)-N-(3,5-DINITROBENZOYL) NOREPHEDRINE BONDED TO SILICA-GEL AS A CHIRAL STATIONARY PHASE FOR THE LIQUID-CHROMATOGRAPHIC SEPARATION OF ENANTIOMERS
HYUN, MH
KIM, MH
[J]. JOURNAL OF LIQUID CHROMATOGRAPHY, 1990, 13 (16): : 3229 - 3243
[9] KANDRA L, 1984, J INCLUSION PHENOM, V2, P869
[10] KONIG WA, 1990, HRC-J HIGH RES CHROM, V13, P702

← 1 2 3 4 →