13C assignments of the carbon atoms in the aromatic rings of lignin model compounds of the arylglycerol β-aryl ether type

被引:16
作者
Bardet, Michel
Lundquist, Knut
Parkas, Jim [1 ]
Robert, Danielle
von Unge, Sverker
机构
[1] Chalmers Univ Technol, Dept Chem Engn & Environm Sci, SE-41296 Gothenburg, Sweden
[2] CEA Grenoble, Dept Rech Fondamentale Mat Condensee, SCIB, F-38041 Grenoble 9, France
[3] CNRS, CERMAV, F-38041 Grenoble 9, France
[4] AstraZeneca R&D Molndal, Med Chem, SE-43183 Molndal, Sweden
关键词
NMR; C-13; lignins; lignin models; arylglycerol beta-aryl ethers;
D O I
10.1002/mrc.1877
中图分类号
O6 [化学];
学科分类号
0703 ;
摘要
The C-13 NMR signals from the aromatic ring carbons in a series of lignin model compounds of the arylglycerol beta-aryl ether type in DMSO solution have been assigned. The model compounds investigated are representative of the erythro and threo forms of differently substituted arylglycerol. beta-aryl ethers. Copyright (c) 2006 John Wiley & Sons, Ltd.
引用
收藏
页码:976 / 979
页数:4
相关论文
共 13 条
[1]   Identification of side-chain structures in a poplar lignin using three-dimensional HMQC-HOHAHA NMR spectroscopy [J].
Ämmälahti, E ;
Brunow, G ;
Bardet, M ;
Robert, D ;
Kilpeläinen, I .
JOURNAL OF AGRICULTURAL AND FOOD CHEMISTRY, 1998, 46 (12) :5113-5117
[2]  
Bardet M, 1998, MAGN RESON CHEM, V36, P597, DOI 10.1002/(SICI)1097-458X(199808)36:8<597::AID-OMR345>3.3.CO
[3]  
2-7
[4]   A COMPARISON OF SOLUTION AND SOLID-STATE C-13 NMR-SPECTRA OF LIGNINS AND LIGNIN MODEL COMPOUNDS [J].
HAWKES, GE ;
SMITH, CZ ;
UTLEY, JHP ;
VARGAS, RR ;
VIERTLER, H .
HOLZFORSCHUNG, 1993, 47 (04) :302-312
[5]   erythro-2-(2,6-dimethoxy-4-methylphenoxy)-1-(4-hydroxy-3,5-dimethoxyphenyl)propane-1,3-diol [J].
Langer, V ;
Lundquist, K ;
Miksche, GE .
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2005, 61 :O1001-O1003
[6]   threo-2-(2,6-Dimethoxyphenoxy)-1-(3,4-dimethoxy-phenyl)-1,3-propanediol [J].
Langer, V ;
Lundquist, K ;
Stomberg, R ;
von Unge, S .
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2002, 58 :o90-o92
[7]   threo-1-(3,4-Dimethoxyphenyl)-2-(2-methoxy-phenoxy)-1,3-propanediol [J].
Langer, V ;
Lundquist, K .
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2002, 58 :O433-O435
[8]   erythro-2-(2,6-Dimethoxyphenoxy)-1-(3,4,5-tri-methoxyphenyl)-1,3-propanediol [J].
Langer, V ;
Lundquist, K .
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2001, 57 :O1219-O1221
[9]  
Leary G. J., 1992, METHODS LIGNIN CHEM, P146
[10]   BEHAVIOR OF LIGNIN IN ALKALINE COOKING .9. ALKALINE DEGRADATION OF ARYLGLYCERINE BETA (2,6-DIMETHOXY-4-ALKYLARYL) ETHER STRUCTURES [J].
MIKSCHE, GE .
ACTA CHEMICA SCANDINAVICA, 1973, 27 (04) :1355-1368