Microstructural investigations on zirconium oxide-carbon nanotube composites synthesized by hydrothermal crystallization

被引：99

作者：

Lupo, F ^{[1
]}

Kamalakaran, R ^{[1
]}

Scheu, C ^{[1
]}

Grobert, N ^{[1
]}

Rühle, M ^{[1
]}

机构：

[1] Max Planck Inst Met Res, D-70569 Stuttgart, Germany

来源：

CARBON | 2004年 / 42卷 / 10期

关键词：

carbon nanotubes; pyrolysis; hydrothermal treatment; transmission electron microscopy; microstructure;

D O I：

10.1016/j.carbon.2004.03.037

中图分类号：

O64 [物理化学（理论化学）、化学物理学];

学科分类号：

070304 ; 081704 ;

摘要：

Zirconium oxide (ZrO2)/carbon nanotube composites were prepared by hydrothermal crystallization at 200 degreesC for 8 h of zirconium hydroxide [(Zr(OH)(4)nH(2)O; n = 8-16] in the presence of carbon nanotubes. The hydrothermal crystallization of zirconium oxide, under autoclave conditions, occurred on the walls of the tubes. The process yielded a homogeneous composite powder consisting of microcrystalline ZrO2 and multi-walled nanotubes, hence representing an alternative route for the synthesis of ceramic-nanotube composites. Microstructural and qualitative characterizations were performed using different electron microscopy techniques. (C) 2004 Elsevier Ltd. All rights reserved.

引用

页码：1995 / 1999

页数：5

共 24 条

[1] Bai JB, 2002, ADV ENG MATER, V4, P701, DOI 10.1002/1527-2648(20020916)4:9<701::AID-ADEM701>3.0.CO
[2] 2-T
[3] Carbon nanotubes - the route toward applications
Baughman, RH
Zakhidov, AA
de Heer, WA
[J]. SCIENCE, 2002, 297 (5582) : 787 - 792
[4] Excellent wave absorption by zirconium-based bulk metallic glass composites containing carbon nanotubes
Bian, Z
Wang, RJ
Pan, MX
Zhao, DQ
Wang, WH
[J]. ADVANCED MATERIALS, 2003, 15 (7-8) : 616 - 621
[5] Carbon-nanotube-reinforced Zr52.5Cu17.9Ni14.6Al10Ti5 bulk metallic glass composites
Bian, Z
Pan, MX
Zhang, Y
Wang, WH
[J]. APPLIED PHYSICS LETTERS, 2002, 81 (25) : 4739 - 4741
[6] Carbon nanotubes: opportunities and challenges
Dai, HJ
[J]. SURFACE SCIENCE, 2002, 500 (1-3) : 218 - 241
[7] Carbon nanotube-metal-oxide nanocomposites:: Microstructure, electrical conductivity and mechanical properties
Flahaut, E
Peigney, A
Laurent, C
Marlière, C
Chastel, F
Rousset, A
[J]. ACTA MATERIALIA, 2000, 48 (14) : 3803 - 3812
[8] Surface modified multi-walled carbon nanotubes in CNT/epoxy-composites
Gojny, FH
Nastalczyk, J
Roslaniec, Z
Schulte, K
[J]. CHEMICAL PHYSICS LETTERS, 2003, 370 (5-6) : 820 - 824
[9] A novel route to aligned nanotubes and nanofibres using laser-patterned catalytic substrates
Grobert, N
Terrones', M
Trasobares, S
Kordatos, K
Terrones, H
Olivares, J
Zhang, JP
Redlich, P
Hsu, WK
Reeves, CL
Wallis, DJ
Zhu, YQ
Hare, JP
Pidduck, AJ
Kroto, HW
Walton, DRM
[J]. APPLIED PHYSICS A-MATERIALS SCIENCE & PROCESSING, 2000, 70 (02): : 175 - 183
[10] HELICAL MICROTUBULES OF GRAPHITIC CARBON
IIJIMA, S
[J]. NATURE, 1991, 354 (6348) : 56 - 58

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