Growth of belt-like SnS crystals from ethylenediamine solution

被引：69

作者：

An, CH

Tang, KB ^{[1
]}

Shen, GZ

Wang, CR

Yang, Q

Hai, B

Qian, YT

机构：

[1] Univ Sci & Technol China, Dept Chem, Hefei 230026, Anhui, Peoples R China

[2] Univ Sci & Technol China, Struct Res Lab, Hefei 230026, Anhui, Peoples R China

来源：

JOURNAL OF CRYSTAL GROWTH | 2002年 / 244卷 / 3-4期

基金：

中国国家自然科学基金;

关键词：

crystal morphology; growth from solutions; semiconducting materials;

D O I：

10.1016/S0022-0248(02)01613-5

中图分类号：

O7 [晶体学];

学科分类号：

0702 ; 070205 ; 0703 ; 080501 ;

摘要：

Tin (II) sulfide crystal belts, with tens of micrometers in width, several millimeters in length and several micrometers in thickness, was successfully grown in ethylenediamine (en) via a solvothermal route at low temperature. The products were characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM), induced-coupled plasma (ICP), X-ray photoelectron spectra (XPS). The vibrational property of the as-prepared SnS belt was examined by Raman spectra. The possible growth mechanism of SnS crystal belts was discussed, which revealed that the solvent (en) was crucial in the formation of belt-like SnS crystals. (C) 2002 Elsevier Science B.V. All rights reserved.

引用

页码：333 / 338

页数：6

共 28 条

[1] THE PREPARATION AND THE ELECTRICAL AND OPTICAL PROPERTIES OF SNS CRYSTALS [J].