Polymer-assisted hydrothermal synthesis of single crystal Pb1-xLaxTiO3 nanorods

被引:7
作者
Deng, Y. [1 ,2 ]
Zhou, J. X. [3 ]
Du, Y. L. [4 ]
Zhu, K. R. [5 ,6 ]
Hu, Y. [1 ,2 ]
Wu, D. [1 ,2 ]
Zhang, M. S. [1 ,2 ]
Du, Y. W. [1 ,2 ]
机构
[1] Nanjing Univ, Natl Lab Solid State Microstruct, Nanjing 210093, Peoples R China
[2] Nanjing Univ, Ctr Mat Anal, Nanjing 210093, Peoples R China
[3] Nanjing Univ Aeronaut & Astronaut, Inst Nanosci, Nanjing 210016, Peoples R China
[4] Nanjing Univ Sci & Technol, Dept Mat Sci & Engn, Nanjing 210094, Peoples R China
[5] Anhui Univ, Sch Phys & Mat Sci, Hefei 230039, Peoples R China
[6] Anhui Univ, Modern Expt Technol Ctr, Hefei 230039, Peoples R China
基金
中国国家自然科学基金;
关键词
Nanorods; Doping; Phonon characteristics; Fabrication and characterization; PBTIO3; PHASE;
D O I
10.1016/j.matlet.2009.01.043
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
Single-crystal PbxLa1-xTiO3 (PLT) nanorods of various La concentrations have been synthesized by polymer-assisted hydrothermal method. The nanorods have diameters of 25-60 nm and average lengths of 3 pm. With tetragonal lattices structures, the PLT nanorods grow along the (001) direction. As La concentration increasing, the tetragonality c/a decreases and the Raman mode E(1TO) becomes softening. PLT nanorods with various lengths and diameters have been prepared by using different polymer additives. To fabricate well-crystallized nanorods, an annealing process after the hydrothermal treatment is proved to be necessary. (C) 2009 Elsevier B.V. All rights reserved.
引用
收藏
页码:937 / 939
页数:3
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