Towards flexible inorganic "mesomaterials": one-pot low temperature synthesis of mesostructured nanocrystalline titania

被引:52
作者
Haseloh, S
Choi, SY
Mamak, M
Coombs, N
Petrov, S
Chopra, N
Ozin, GA
机构
[1] Univ Toronto, Dept Chem, Mat Chem Res Grp, Toronto, ON M5S 3H6, Canada
[2] Xerox Res Ctr Canada Ltd, Mississauga, ON L5K 2L1, Canada
关键词
D O I
10.1039/b403607g
中图分类号
O6 [化学];
学科分类号
0703 ;
摘要
We hereby report a simple route for the low temperature synthesis of mesoporous nanocrystalline titania involving brief hydrothermal treatment of butanolic precursors and non-ionic tri-block-copolymer surfactant at 100 degreesC, followed by evaporation induced self assembly to make a crack-free flexible film. At no time in the film-forming process is a temperature of more than 120 degreesC reached, thereby permitting the use of substrates that are not stable to higher temperatures.
引用
收藏
页码:1460 / 1461
页数:2
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