Electrosynthesis of α-arylated β-substituted cyclopropylphosphonates.: Synthesis of a phosphonic analogue of minalcipran

被引:26
作者
Duquenne, C
Goumain, S
Jubault, P
Feasson, C
Quirion, JC
机构
[1] INSA, IRCOF, CNRS, Lab Heterochim Organ, F-76130 Mt St Aignan, France
[2] Univ Rouen, F-76130 Mt St Aignan, France
关键词
D O I
10.1021/ol991301k
中图分类号
O62 [有机化学];
学科分类号
070303 ; 081704 ;
摘要
[GRAPHICS] The synthesis of alpha-arylated beta-substituted cyclopropylphosphonates was efficiently achieved by electroreduction of diethyl alpha,alpha-dichlorobenzylphosphonate in the presence of Michael accepters in a one compartment cell equipped with a magnesium sacrificial anode.
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页码:453 / 455
页数:3
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