Synthesis and X-ray analysis of 1-((1S)-phenylethyl)-azetidine-(2R)-piperidinamide

被引：3

作者：

deGelder, R ^{[1
]}

Smits, JMM ^{[1
]}

Starmans, WAJ ^{[1
]}

Thijs, L ^{[1
]}

Zwanenburg, B ^{[1
]}

机构：

[1] CATHOLIC UNIV NIJMEGEN,NIJMEGEN SON RES CTR,DEPT ORGAN CHEM,NL-6525 ED NIJMEGEN,NETHERLANDS

来源：

JOURNAL OF CHEMICAL CRYSTALLOGRAPHY | 1996年 / 26卷 / 09期

关键词：

crystal structure; chiral auxiliaries;

D O I：

10.1007/BF01668624

中图分类号：

O7 [晶体学];

学科分类号：

0702 ; 070205 ; 0703 ; 080501 ;

摘要：

The crystal and molecular structure of a new azetidine-2-carboxylic amide derivative is described. The structure was solved by direct methods and refined by least squares methods to R1 = 0.0393 for 4264 reflections (with I > 2 sigma(I)). The structure consists of two independent molecules which are chemically the same with slight differences in geometry. Crystal data: C17H24N2O, monoclinic, space group P2(1), a = 8.3782(4), b = 20.0342(13), c = 9.7769(8)Angstrom, beta = 109.687(6)degrees, V = 1545.1(2)Angstrom(3), Z = 4.

引用

页码：639 / 642

页数：4

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