Determination of polybrominated diphenyl ethers in soil from e-waste recycling site

被引：96

作者：

Cai, Zongwei ^{[1
]}

Jiang, Guibin

机构：

[1] Hong Kong Baptist Univ, Dept Chem, Kowloon, Hong Kong, Peoples R China

[2] Chinese Acad Sci, Ecoenvironm Sci Res Ctr, Beijing, Peoples R China

来源：

TALANTA | 2006年 / 70卷 / 01期

基金：

中国国家自然科学基金;

关键词：

PBDEs; e-waste; soil; GC-ion trap MS;

D O I：

10.1016/j.talanta.2006.01.016

中图分类号：

O65 [分析化学];

学科分类号：

070302 ; 081704 ;

摘要：

Soil samples collected from an electronic waste recycling site were prepared by using Soxhlet extraction and multiple-step column chromatographic clean-up. Gas chromatography/ion trap mass spectrometry method was developed to determine polybrominated diphenyl ethers (PBDEs) in the sample extracts. The method performance was evaluated by the recovery of 13 C-labeled internal standards and by analyzing quality assurance and quality control samples. Relative error and relative standard deviation obtained from the analysis of duplicated samples and spiked matrix were better than 10%. PBDEs were detected in the field soil samples collected from an e-wastes disposal site at levels from low parts-per-bill ions to 600 parts-per-bill ions. (c) 2006 Elsevier B.V. All rights reserved.

引用

页码：88 / 90

页数：3

共 12 条

[1] A gas chromatography/high-resolution mass spectrometry (GC/HRMS) method for determination of polybrominated diphenyl ethers in fish
Alaee, M
Sergeant, DB
Ikonomou, MG
Luross, JM
[J]. CHEMOSPHERE, 2001, 44 (06) : 1489 - 1495
[2] Polybrominated dibenzo-p-dioxins, dibenzofurans, and diphenyl ethers in Japanese human adipose tissue
Choi, JW
Fujimaki, S
Kitamura, K
Hashimoto, S
Ito, H
Suzuki, N
Sakai, S
Morita, M
[J]. ENVIRONMENTAL SCIENCE & TECHNOLOGY, 2003, 37 (05) : 817 - 821
[3] An overview of brominated flame retardants in the environment
de Wit, CA
[J]. CHEMOSPHERE, 2002, 46 (05) : 583 - 624
[4] IMMUNOLOGICAL AND ENDOCRINE EFFECTS OF THE FLAME-RETARDANT PENTABROMODIPHENYL ETHER (DE-71) IN C57BL/6J MICE
FOWLES, JR
FAIRBROTHER, A
BAECHERSTEPPAN, L
KERKVLIET, NI
[J]. TOXICOLOGY, 1994, 86 (1-2) : 49 - 61
[5] Supercritical fluid extraction with solid-phase trapping of chlorinated and brominated pollutants from sediment samples
Hartonen, K
Bowadt, S
Hawthorne, SB
Riekkola, ML
[J]. JOURNAL OF CHROMATOGRAPHY A, 1997, 774 (1-2) : 229 - 242
[6] Determination of brominated flame retardants in environmental samples
Hyötyläinen, T
Hartonen, K
[J]. TRAC-TRENDS IN ANALYTICAL CHEMISTRY, 2002, 21 (01) : 13 - 29
[7] Occurrence and specific congener profile of 40 polybrominated diphenyl ethers in river and coastal sediments from Portugal
Lacorte, S
Guillamón, M
Martínez, E
Viana, P
Barceló, D
[J]. ENVIRONMENTAL SCIENCE & TECHNOLOGY, 2003, 37 (05) : 892 - 898
[8] Potent competitive interactions of some brominated flame retardants and related compounds with human transthyretin in vitro
Meerts, IATM
van Zanden, JJ
Luijks, EAC
van Leeuwen-Bol, I
Marsh, G
Jakobsson, E
Bergman, Å
Brouwer, A
[J]. TOXICOLOGICAL SCIENCES, 2000, 56 (01) : 95 - 104
[9] PBCDD and PBCDF from incineration of waste-containing brominated flame retardants
Söderström, G
Marklund, S
[J]. ENVIRONMENTAL SCIENCE & TECHNOLOGY, 2002, 36 (09) : 1959 - 1964
[10] Concentrations and spatial variations of polybrominated diphenyl ethers and other organohalogen compounds in Great Lakes air
Strandberg, B
Dodder, NG
Basu, I
Hites, RA
[J]. ENVIRONMENTAL SCIENCE & TECHNOLOGY, 2001, 35 (06) : 1078 - 1083

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