Development of a filtration and titration method for the determination of the acidity of humic acids.

被引:17
作者
Prado, AGS [1 ]
Souza, SM [1 ]
da Silva, WTL [1 ]
Rezende, MOD [1 ]
机构
[1] Univ Sao Paulo, Inst Quim Sao Carlos, BR-13560970 Sao Carlos, SP, Brazil
来源
QUIMICA NOVA | 1999年 / 22卷 / 06期
关键词
humic acids; acidity; titration method;
D O I
10.1590/S0100-40421999000600018
中图分类号
O6 [化学];
学科分类号
0703 ;
摘要
The acidity determinations method of humic acids (HA) content was developed by Schnitzer and Gupta and is a very well known procedure. Nevertheless, care is necessary to prevent measure errors due to non-controlled BaCO3 production, during the filtration and titration of HA total acidity, To overcome this problem, we developed in our laboratory a simple filtration and titration system for the determination of HA acidity under inert atmosphere. This system enables a better reproducibility and accuracy of total, carboxylic and phenolic acidity measures than those by Schnitzer and Gupta method.
引用
收藏
页码:894 / 896
页数:3
相关论文
共 8 条
[1]  
BARROS MCP, 1994, QUIM NOVA, V17, P376
[2]   LABILE/INERT METAL SPECIES IN AQUATIC HUMIC SUBSTANCES - AN ION-EXCHANGE STUDY [J].
BURBA, P .
FRESENIUS JOURNAL OF ANALYTICAL CHEMISTRY, 1994, 348 (04) :301-311
[3]   CELLULOSE TETPA - A CHELATING COLLECTOR DESIGNED FOR MULTIELEMENT PRECONCENTRATION IN FLOW SYSTEMS [J].
BURBA, P ;
ROCHA, JC ;
SCHULTE, A .
FRESENIUS JOURNAL OF ANALYTICAL CHEMISTRY, 1993, 346 (04) :414-419
[4]   LABILE COMPLEXES OF TRACE-METALS IN AQUATIC HUMIC SUBSTANCES - INVESTIGATIONS BY MEANS OF AN ION EXCHANGE-BASED FLOW PROCEDURE [J].
BURBA, P ;
ROCHA, J ;
KLOCKOW, D .
FRESENIUS JOURNAL OF ANALYTICAL CHEMISTRY, 1994, 349 (12) :800-807
[5]   STRUCTURAL INVESTIGATIONS OF HUMIC-ACID FROM LEONARDITE BY SPECTROSCOPIC METHODS AND THERMAL-ANALYSIS [J].
RICCA, G ;
FEDERICO, L ;
ASTORI, C ;
GALLO, R .
GEODERMA, 1993, 57 (03) :263-274
[6]   ALKALI VERSUS ACID EXTRACTION OF SOIL ORGANIC MATTER [J].
SCHNITZER, M ;
SKINNER, SIM .
SOIL SCIENCE, 1968, 105 (06) :392-+
[7]  
SCHNITZER M., 1965, SOIL SCI SOC AMER PROC, V29, P274
[8]   COPPER(II) AND IRON(III) COMPLEXATION BY SOIL HUMIC ACIDS - AN IR AND ELECTRON-SPIN-RESONANCE STUDY [J].
SENESI, N ;
SPOSITO, G ;
MARTIN, JP .
SCIENCE OF THE TOTAL ENVIRONMENT, 1986, 55 :351-362