Temperature, heat and heat flow rate calibration of differential scanning calorimeters

被引：56

作者：

Gmelin, E

Sarge, SM

机构：

[1] Max Planck Inst Festkorperforsch, D-70569 Stuttgart, Germany

[2] Phys Tech Bundesanstalt, D-38116 Braunschweig, Germany

来源：

THERMOCHIMICA ACTA | 2000年 / 347卷 / 1-2期

关键词：

differential scanning calorimeters; calibration of DSC; calibration of temperature; heat calibration; heat flow rate calibration;

D O I：

10.1016/S0040-6031(99)00424-4

中图分类号：

O414.1 [热力学];

学科分类号：

摘要：

This contribution discusses basic problems and fundamental requirements for a universally applicable, unified and metrologically correct calibration of differential scanning calorimeters (DSC). The essential features of previously published recommendations of the German Society for Thermal Analysis (GEFTA) [see Hohne et al., Thermochim. Acta 160 (1990) 112; Cammenga et al., Thermochim. Acta 219 (1993) 333-343; Sarge et al., Thermochim. Acta 247 (1994) 129-168; J. Thermal Anal. 49 (1997) 1125-1134] developed for a correct and instrument-independent calibration of temperature, heat and heat flow rate of DSC, are outlined. (C) 2000 Elsevier Science B.V. All rights reserved.

引用

页码：9 / 13

页数：5

共 19 条

[1] DEVELOPMENT OF STANDARD OPERATING PROCEDURES FOR DIFFERENTIAL SCANNING CALORIMETERS [J].