Synthesis and studies of growth kinetics of monodispersed iron oxide nanoparticles using ferrocene as novel precursor

被引：11

作者：

Bhalerao, G. M. ^{[1
]}

Sinha, A. K. ^{[1
]}

Srivastava, Himanshu ^{[1
]}

Srivastava, A. K. ^{[1
]}

机构：

[1] Raja Ramanna Ctr Adv Technol, Ind Synchrotrons Utilizat Div, Indore 452013, India

来源：

APPLIED PHYSICS A-MATERIALS SCIENCE & PROCESSING | 2009年 / 95卷 / 02期

关键词：

CARBON NANOTUBES;

D O I：

10.1007/s00339-008-5068-z

中图分类号：

T [工业技术];

学科分类号：

120111 [工业工程];

摘要：

We have used ferrocene and paraffin wax as novel precursor and solvent for the growth of iron oxide nanoparticles. The proposed method of growth has several advantages over existing methods of growth using iron pentacarbonyl a precursor. Highly crystalline and monodispersed particles are obtained which assemble in two- and three-dimensional hexagonal closed packed superlattices. Growth kinetics has been studied by varying concentration of the precursor and time of growth. A phenomenological model has been proposed to explain the growth kinetics.

引用

页码：373 / 380

页数：8

共 21 条

[1]

Growth of double-wall carbon nanotubes with diameter-controlled iron oxide nanoparticles supported on MgO [J].

Ago, H ;

Nakamura, K ;

Imamura, S ;

Tsuji, M .

CHEMICAL PHYSICS LETTERS, 2004, 391 (4-6) :308-313

[2]

[Anonymous], MAT SAFETY DATA SHEE

[3]

Synthesis of Monodispersed γ-Fe2O3 Nanoparticles Using Ferrocene as a Novel Precursor [J].

Bhalerao, G. M. ;

Sinha, A. K. ;

Srivastava, A. K. .

JOURNAL OF NANOSCIENCE AND NANOTECHNOLOGY, 2009, 9 (09) :5502-5506

[4]

Synthesis and properties of iron ferrofluids [J].

Butter, K ;

Philipse, AP ;

Vroege, GJ .

JOURNAL OF MAGNETISM AND MAGNETIC MATERIALS, 2002, 252 (1-3) :1-3

[5]

The concept of delayed nucleation in nanocrystal growth demonstrated for the case of iron oxide nanodisks [J].

Casula, MF ;

Jun, YW ;

Zaziski, DJ ;

Chan, EM ;

Corrias, A ;

Alivisatos, AP .

JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 2006, 128 (05) :1675-1682

[6]

REACTIVITY OF THE 1ST TRANSITION ROW METALLOCENES IN THERMAL-DECOMPOSITION REACTION [J].

DYAGILEVA, LM ;

MARIN, VP ;

TSYGANOVA, EI .

JOURNAL OF ORGANOMETALLIC CHEMISTRY, 1979, 175 (01) :63-72

[7]

CO hydrogenation over cobalt and iron catalysts supported over multiwall carbon nanotubes:: Effect of preparation [J].

Guczi, Laszlo ;

Stefler, G. ;

Geszti, O. ;

Koppany, Zs. ;

Konya, Z. ;

Molnar, E. ;

Urban, M. ;

Kiricsi, I. .

JOURNAL OF CATALYSIS, 2006, 244 (01) :24-32

[8]

Diameter-controlled synthesis of discrete and uniform-sized single-walled carbon nanotubes using monodisperse iron oxide nanoparticles embedded in zirconia nanoparticle arrays as catalysts [J].

Han, SJ ;

Yu, TK ;

Park, J ;

Koo, B ;

Joo, J ;

Hyeon, T ;

Hong, S ;

Im, J .

JOURNAL OF PHYSICAL CHEMISTRY B, 2004, 108 (24) :8091-8095

[9]

*JCPDS, 251402 JCPDS

[10]

*JCPDS, 391346 JCPDS

← 1 2 3 →