Synthesis of the chiral auxiliary 1,3:4,6-Di-O-benzylidene-2,5-dideoxy-2,5-imino-D-iditol

被引：5

作者：

Giese, B ^{[1
]}

Muller, SN ^{[1
]}

Wyss, C ^{[1
]}

Steiner, H ^{[1
]}

机构：

[1] CIBA GEIGY AG,KATALYSE & SYNTHESEDIENSTE FD6,CH-4002 BASEL,SWITZERLAND

来源：

TETRAHEDRON-ASYMMETRY | 1996年 / 7卷 / 05期

关键词：

D O I：

10.1016/0957-4166(96)00137-1

中图分类号：

O61 [无机化学];

学科分类号：

070301 ; 081704 ;

摘要：

L-Mannitol 5, the precursor of the the C-2-symmetrical auxiliary 3B, was prepared in high yield by heterogeneous reduction of L-mannonic-gamma-lactone 4. The auxiliary 3B could be used for stereoselective photochemical synthesis of the L-proline derivative 2B. Copyright (C) 1996 Elsevier Science Ltd

引用

页码：1261 / 1262

页数：2

共 8 条

[1]

ANANTHARAMAICH GM, 1976, J CHEM SOC P1, P490

[2] Studies on acetone-glyceraldehyde. VII. Preparation of l-glyceraldehyde and l(-)acetone glycerol [J].

Baer, E ;

Fischer, HOL .

JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1939, 61 :761-765

[3] AMINE EXCHANGE REACTIONS - MANNICH BASES FROM PRIMARY ALIPHATIC AMINES AND FROM AMINO ACIDS [J].

CRAIG, JC ;

MOYLE, M ;

JOHNS, SR .

JOURNAL OF ORGANIC CHEMISTRY, 1963, 28 (10) :2779-&

[4]

GLATTFELD JWE, 1927, J AM CHEM SOC, V49, P2306

[5]

KOGYO NK, 1972, Patent No. 2043349

[6]

OTTENHEIJM HCJ, 1983, ORG SYNTH, V61, P1

[7]

STREITH J, 1991, HELV CHIM ACTA, V74, P103

[8] ASYMMETRIC-SYNTHESIS OF 3-HYDROXYPROLINES BY PHOTOCYCLIZATION OF N-(2-BENZOYLETHYL)GLYCINAMIDES [J].

WESSIG, P ;

WETTSTEIN, P ;

GIESE, B ;

NEUBURGER, M ;

ZEHNDER, M .

HELVETICA CHIMICA ACTA, 1994, 77 (03) :829-837

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