Determination of esters in dry and sweet white wines by headspace solid-phase microextraction and gas chromatography

被引：76

作者：

Rodríguez-Bencomo, JJ ^{[1
]}

Conde, JE ^{[1
]}

Rodríguez-Delgado, MA ^{[1
]}

García-Montelongo, F ^{[1
]}

Pérez-Trujillo, JP ^{[1
]}

机构：

[1] Univ La Laguna, Dept Analyt Chem Nutr & Food Sci, San Cristobal la Laguna 38071, Tenerife, Spain

来源：

JOURNAL OF CHROMATOGRAPHY A | 2002年 / 963卷 / 1-2期

关键词：

wine; food analysis; solid-phase microextraction; headspace analysis; esters;

D O I：

10.1016/S0021-9673(02)00551-4

中图分类号：

Q5 [生物化学];

学科分类号：

071010 ; 081704 ;

摘要：

Headspace solid-phase microextraction (HS-SPME) was studied for the high-resolution gas chromatographic (HRGC) analysis of esters in wines. Five different SPME fibers were tested and the influence of different factors such as temperature and time of desorption, extraction time, extraction technique, stirring, sample and vial volume, sugar and ethanol content were studied and optimised using model solutions. The proposed HS-SPME-GC method is an appropriate technique for the quantitative analysis of esters in dry and sweet white wines. (C) 2002 Elsevier Science B.V. All rights reserved.

引用

页码：213 / 223

页数：11

共 24 条

[1]

[Anonymous], J HIGH RESOLUTION CH

[2] SOLID-PHASE MICROEXTRACTION WITH THERMAL-DESORPTION USING FUSED-SILICA OPTICAL FIBERS [J].

ARTHUR, CL ;

PAWLISZYN, J .

ANALYTICAL CHEMISTRY, 1990, 62 (19) :2145-2148

[3]

De la Calle Garcia D., 1997, J HIGH RES CHROMATOG, V20, P665

[4]

DELACALLE D, 1996, J HIGH RES CHROMATOG, V19, P257

[5]

Fisher C., 1997, J AGR FOOD CHEM, V45, P1995

[6]

Francioli S, 1999, AM J ENOL VITICULT, V50, P404

[7]

Gandini N, 1997, J AGR FOOD CHEM, V45, P3092, DOI 10.1021/jf960441v

[8]

GARCIA MJ, 1999, NOV ALIMENT, P83

[9] Identification of character impact odorants of different white wine varieties [J].

Guth, H .

JOURNAL OF AGRICULTURAL AND FOOD CHEMISTRY, 1997, 45 (08) :3022-3026

[10] Analysis of diacetyl in wine using solid-phase microextraction combined with gas chromatography mass spectrometry [J].

Hayasaka, Y ;

Bartowsky, EJ .

JOURNAL OF AGRICULTURAL AND FOOD CHEMISTRY, 1999, 47 (02) :612-617

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