Paris-Edinburgh large-volume cell coupled with a fast imaging-plate system for structural investigation at high pressure and high temperature

被引:64
作者
Mezouar, M [1 ]
Le Bihan, T [1 ]
Libotte, H [1 ]
Le Godec, Y [1 ]
Häusermann, D [1 ]
机构
[1] European Synchrotron Radiat Facil, F-38000 Grenoble, France
来源
JOURNAL OF SYNCHROTRON RADIATION | 1999年 / 6卷
关键词
high pressure; high temperature; Paris-Edinburgh cell; image plates; Rietveld refinement; InSb; BN;
D O I
10.1107/S0909049599010651
中图分类号
TH7 [仪器、仪表];
学科分类号
0804 ; 080401 ; 081102 ;
摘要
A new set-up for collecting high-quality data suitable for structural refinement at high pressure and high temperature has been developed on beamline ID30 at the ESRF The possibility of using high X-ray energies, high brilliance of third-generation sources and a new fast imaging-plate detector interfaced to the Paris-Edinburgh large-volume press has lead to a significant reduction of acquisition time and improvement of the quality of the data. The feasibility of angle-dispersive X-ray diffraction experiments at high pressure and high temperature, even on light elements, has been demonstrated.
引用
收藏
页码:1115 / 1119
页数:5
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