Pore structure characterization of mesoporous/microporous materials by H-1 NMR using water as a probe molecule

被引：34

作者：

Hansen, EW ^{[1
]}

Tangstad, E ^{[1
]}

Myrvold, E ^{[1
]}

Myrstad, T ^{[1
]}

机构：

[1] STATOIL, R&D CTR POSTUTTAK, N-7005 TRONDHEIM, NORWAY

来源：

JOURNAL OF PHYSICAL CHEMISTRY B | 1997年 / 101卷 / 50期

关键词：

D O I：

10.1021/jp9721964

中图分类号：

O64 [物理化学（理论化学）、化学物理学];

学科分类号：

070304 ; 081704 ;

摘要：

Model improvements related to the analysis of H-1 NMR signal intensity vs temperature (IT-curve) of a fluid confined in porous materials are presented enabling pore size distribution, specific surface area, and relative distribution of pore volumes to be extracted. The model is applied to four different porous materials, two containing mesopores only and two containing both mesopores and micropores.

引用

页码：10709 / 10714

页数：6

共 13 条

[1]

ABRAGAM A, 1961, PRINCIPLES NUCLEAR M

[2]

AKPORIAYE D, 1993, J PHYS CHEM-US, V97, P7743

[3] STUDY OF HF DOPED ICE BY PULSED NMR [J].