Hydrothermal synthesis of monodisperse CeO2 nanocubes

被引：52

作者：

Yang, Zhijie ^{[1
]}

Yang, Yanzhao ^{[1
]}

Liang, Hui ^{[1
]}

Liu, Ling ^{[1
]}

机构：

[1] Shandong Univ, Sch Chem & Chem Engn, Jinan 250100, Shandong, Peoples R China

来源：

MATERIALS LETTERS | 2009年 / 63卷 / 21期

关键词：

Crystal growth; Nanomaterials; Monodisperse; CeO2; SHAPE-CONTROLLED SYNTHESIS; NANOPARTICLES; MORPHOLOGY; SILVER; WATER; NANOSPHERES; CERIUM(IV); PARTICLES; GAS;

D O I：

10.1016/j.matlet.2009.05.034

中图分类号：

T [工业技术];

学科分类号：

08 ;

摘要：

Monodisperse CeO2 nanocubes have been fabricated via an acrylamide-assisted hydrothermal route. NH3 and acrylic acid from the hydrolysis of acrylamide act as OH- provider and capping reagent, respectively. The structure and morphology of the products were characterized by X-ray diffraction (XRD), transmission electron microscopy (TEM), high-resolution transmission electron microscopy (HRTEM), field-emission scanning electron microscopy (FE-SEM) and Fourier transformed infrared (FT-IR). The products have a cubic morphology with a mean size of 200 nm. The possible formation mechanism has been discussed based on the experimental results. (C) 2009 Elsevier B.V. All rights reserved.

引用

页码：1774 / 1777

页数：4

共 21 条

[1]

CARUSO F, 1997, NATURE, V386, P143

[2] Monodisperse magnetic single-crystal ferrite microspheres [J].

Deng, H ;

Li, XL ;

Peng, Q ;

Wang, X ;

Chen, JP ;

Li, YD .

ANGEWANDTE CHEMIE-INTERNATIONAL EDITION, 2005, 44 (18) :2782-2785

[3] Preparation and characterization of ceria nanospheres by microwave-hydrothermal method [J].

Dos Santos, M. L. ;

Lima, R. C. ;

Riccardi, C. S. ;

Tranquilin, R. L. ;

Bueno, P. R. ;

Varela, J. A. ;

Longo, E. .

MATERIALS LETTERS, 2008, 62 (30) :4509-4511

[4] Novel synthesis of nanocrystalline CeO2 by mechanochemical and water-in-oil microemulsion methods [J].

Hadi, Abdul ;

Yaacob, Iskandar Idris .

MATERIALS LETTERS, 2007, 61 (01) :93-96

[5] Polyol synthesis of platinum nanoparticles: Control of morphology with sodium nitrate [J].

Herricks, T ;

Chen, JY ;

Xia, YN .

NANO LETTERS, 2004, 4 (12) :2367-2371

[6] Morphology-controllable synthesis of mesoporous CeO2 nano- and microstructures [J].

Ho, CM ;

Yu, JC ;

Kwong, T ;

Mak, AC ;

Lai, SY .

CHEMISTRY OF MATERIALS, 2005, 17 (17) :4514-4522

[7] PREPARATION AND PROPERTIES OF MONODISPERSED COLLOIDAL PARTICLES OF LANTHANIDE COMPOUNDS .2. CERIUM(IV) [J].

HSU, WP ;

RONNQUIST, L ;

MATIJEVIC, E .

LANGMUIR, 1988, 4 (01) :31-37

[8] Large-scale synthesis of silver nanocubes: The role of HCl in promoting cube perfection and monodispersity [J].

Im, SH ;

Lee, YT ;

Wiley, B ;

Xia, YN .

ANGEWANDTE CHEMIE-INTERNATIONAL EDITION, 2005, 44 (14) :2154-2157

[9] Shape-selective synthesis and oxygen storage behavior of ceria nanopolyhedra, nanorods, and nanocubes [J].

Mai, HX ;

Sun, LD ;

Zhang, YW ;

Si, R ;

Feng, W ;

Zhang, HP ;

Liu, HC ;

Yan, CH .

JOURNAL OF PHYSICAL CHEMISTRY B, 2005, 109 (51) :24380-24385

[10] Characterization of Cerium(IV) oxide ultrafine particles prepared using reversed micelles [J].

Masui, T ;

Fujiwara, K ;

Machida, K ;

Adachi, G ;

Sakata, T ;

Mori, H .

CHEMISTRY OF MATERIALS, 1997, 9 (10) :2197-2204

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